1-(4-吗啉)-2-苯基乙烷硫酮合成路线 (共 33 条)
反应条件
tetraphosphorus decasulfide in dichloromethane
Substitution; 5 h; Heating;
参考文献
Heyde, Cornelia; Zug, Ines; Hartmann, Horst
European Journal of Organic Chemistry, 2000 , # 19 p. 3273 - 3278
反应条件
sulfur
Willgerodt-Kindler reaction; 0.0666667 h; microwave irradiation;
参考文献
Darabi, Hossein Reza; Aghapoor, Kioumars; Tabar-Heydar, Kourosh; Nooshabadi, Masoud
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1189 - 1192
反应条件
FeBr2 in dimethyl sulfoxide
T=50°C;
参考文献
Murguia, Marcelo C.; Rossi, Roberto A.
Tetrahedron Letters, 1997 , vol. 38, # 8 p. 1355 - 1358
反应条件
in methanol
72 h; Ambient temperature;
参考文献
Ogura, Katsuyuki; Ito, Yoko; Tsuchihashi, Gen-ichi
Synthesis, 1980 , # 9 p. 736 - 739
参考文献
Campaigne; Rutan
Journal of the American Chemical Society, 1947 , vol. 69, p. 1211
反应条件
sulfur
Willgerodt-Kindler reaction; 0.0666667 h; microwave irradiation;
参考文献
Darabi, Hossein Reza; Aghapoor, Kioumars; Tabar-Heydar, Kourosh; Nooshabadi, Masoud
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1189 - 1192
反应条件
1: t-BuOK / dimethylsulfoxide
2: 87 percent Chromat. / FeBr2 / dimethylsulfoxide / 50 °C
View Scheme
参考文献
Murguia, Marcelo C.; Rossi, Roberto A.
Tetrahedron Letters, 1997 , vol. 38, # 8 p. 1355 - 1358
反应条件
sulfur
T=100°C; Willgerodt-Kindler reaction; 3 h;
参考文献
Darabi, Hossein Reza; Aghapoor, Kioumars; Tajbakhsh, Mahmoud
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4167 - 4169
反应条件
sulfur
Willgerodt-Kindler reaction; 0.0666667 h; microwave irradiation;
参考文献
Darabi, Hossein Reza; Aghapoor, Kioumars; Tabar-Heydar, Kourosh; Nooshabadi, Masoud
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 5 p. 1189 - 1192
反应条件
1: 11 h / 110 °C
2: 77 percent / methanol / 72 h / Ambient temperature
View Scheme
参考文献
Ogura, Katsuyuki; Ito, Yoko; Tsuchihashi, Gen-ichi
Synthesis, 1980 , # 9 p. 736 - 739