1: 68 percent / N-bromosuccinimide / 2 h / Ambient temperature 2: 74 percent / KO-t-Bu / 2-methyl-propan-2-ol / 0.5 h / Heating 3: 1.) O3, 2.) dimethyl sulfide / 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, RT, 12 h 4: 1.) KH / 1.) THF, RT, 2.) THF, from -78 deg C to RT 5: 83 percent / aq. NaOH / 48 h View Scheme
参考文献
Kirby, Anthony J.; Williams, Nicholas H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 4 p. 643 - 648
Bruson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2457,2459
Journal of the American Chemical Society, 1944 , vol. 66, p. 2135
Full Text Show Details
Dressler; Kurland
Journal of Organic Chemistry, 1964 , vol. 29, p. 175,177
Resinous Prod. and Chem. Co.
Patent: US2339218 , 1941 ;
Full Text Show Details
Resinous Prod. and Chem. Co.
Patent: US2280058 , 1941 ;
Full Text Show Details
Bruson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2457,2459
Journal of the American Chemical Society, 1944 , vol. 66, p. 2135