您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻吩
合成路线
（共 462 条）
7450-03-5
+
95-15-8
苯并噻吩
→
反应条件
147619-79-2
+
55084-51-0
反应条件
dichloro bis(acetonitrile) palladium(II); 1,2-dichloro-ethane; copper dichloride T=80°C; 16 h; Inert atmosphere; Overall yield = 19 percent; Overall yield = 21 mg; regioselective reaction;
参考文献
Funaki, Kenji; Sato, Tetsuo; Oi, Shuichi
Organic Letters, 2012 , vol. 14, # 24 p. 6186 - 6189
1003-09-4
+
95-15-8
苯并噻吩
→
反应条件
55164-48-2
反应条件
1: benzo[b]thiophene With n-butyllithium in tetrahydrofuran; hexane T=0°C; 1 h; 2: With tributyltin chloride in tetrahydrofuran; hexane T=20°C; 1 h; 3: thien-2-yl bromide With tetrakis(triphenylphosphine) palladium(0) in toluene Stille reaction; 16 h; Heating;
参考文献
Nicolas, Yohann; Blanchard, Philippe; Levillain, Eric; Allain, Magali; Mercier, Nicolas; Roncali, Jean
Organic Letters, 2004 , vol. 6, # 2 p. 273 - 276
95-15-8
苯并噻吩
→
反应条件
55164-48-2
反应条件
1: 75 percent / n-BuLi; I2 / hexane; tetrahydrofuran / -50 - 20 °C 2: 90 percent / Pd(PPh3)4 / toluene / 20 h / Heating View Scheme
参考文献
Nicolas, Yohann; Blanchard, Philippe; Levillain, Eric; Allain, Magali; Mercier, Nicolas; Roncali, Jean
Organic Letters, 2004 , vol. 6, # 2 p. 273 - 276
95-15-8
苯并噻吩
+
90-13-1
→
反应条件
55712-59-9
反应条件
5 palladium on charcoal; caesium carbonate; copper(l) chloride in 1,4-dioxane T=150°C; 60 h; Sealed tube;
参考文献
Tang, Dan-Tam D.; Collins, Karl D.; Glorius, Frank
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7450 - 7453
2516-40-7
+
95-15-8
苯并噻吩
→
反应条件
596804-30-7
反应条件
1: benzo[b]thiophene With n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: 2-bromobenzothiazole With potassium phosphate; C45H58ClNPPd in tetrahydrofuran; hexane; water T=40°C; Suzuki-Miyaura Coupling; 2 h; Inert atmosphere;
参考文献
Oberli, Matthias A.; Buchwald, Stephen L.
Organic Letters, 2012 , vol. 14, # 17 p. 4606 - 4609
95-16-9
+
95-15-8
苯并噻吩
→
反应条件
596804-30-7
反应条件
1,10-phenanthroline; palladium diacetate; silver nitrate in dimethyl sulfoxide T=110°C; 10 h; Sealed tube;
参考文献
Chen, Xuxing; Huang, Xiaojing; He, Qian; Xie, Yuyuan; Yang, Chunhao
Chemical Communications, 2014 , vol. 50, # 30 p. 3996 - 3999
20637-27-8
+
95-15-8
苯并噻吩
→
反应条件
596804-30-7
反应条件
1,10-phenanthroline; palladium diacetate; silver nitrate in dimethyl sulfoxide T=110°C; 8 h; Sealed tube;
参考文献
Chen, Xuxing; Huang, Xiaojing; He, Qian; Xie, Yuyuan; Yang, Chunhao
Chemical Communications, 2014 , vol. 50, # 30 p. 3996 - 3999
95-15-8
苯并噻吩
→
反应条件
61503-23-9
反应条件
1: 78 percent / aluminium chloride / 0.5 h / 20 °C 2: 100 percent / hyrogen peroxide / acetic acid View Scheme
参考文献
Clark, Peter David; Clarke, Kenneth; Ewing, David F.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 677 - 685
95-15-8
苯并噻吩
→
反应条件
6224-55-1
反应条件
1: butyl lithium; diethyl ether / Behandeln der Reaktionsloesung mit Dimethylsulfat 2: acetic acid; aqueous hydrogen peroxide View Scheme
参考文献
Karaulowa et al.
Doklady Akademii Nauk SSSR, 1958 , vol. 123, p. 99
Doklady Chemistry, 118-123 <1958> 797
95-15-8
苯并噻吩
→
反应条件
6224-56-2
反应条件
1: butyl lithium; diethyl ether / Behandeln der Reaktionsloesung mit Dimethylsulfat 2: acetic acid; aqueous hydrogen peroxide 3: palladium/charcoal / 36775.4 Torr / Hydrogenation View Scheme
参考文献
Karaulowa et al.
Doklady Akademii Nauk SSSR, 1958 , vol. 123, p. 99
Doklady Chemistry, 118-123 <1958> 797
首页
上一页
1
...
41
42
43
44
45
46
47
下一页
末页
到第
页
确定
