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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻唑
合成路线
(共 604 条)
95-16-9
苯并噻唑
+
629-45-8
二丁基二硫
→
反应条件
2314-17-2
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966
95-16-9
苯并噻唑
+
363-72-4
→
反应条件
69200-85-7
+
434-90-2
反应条件
4,4'-dimethoxy-2,2'-bipyridine; di-tert-butyl peroxide; copper(l) chloride; lithium tert-butylate in dichloromethane T=80°C; 10 h; GloveboxSealed tubeInert atmosphere;
参考文献
Fan, Shilu; Zhang, Xingang; Chen, Zhao
Organic Letters, 2012 , vol. 14, # 18 p. 4950 - 4953,4
95-16-9
苯并噻唑
+
363-72-4
+
1907-33-1
→
反应条件
69200-85-7
+
434-90-2
+
1398310-45-6
反应条件
4,4'-dimethoxy-2,2'-bipyridine; di-tert-butyl peroxide; copper(l) chloride in dichloromethane T=80°C; 6 h; GloveboxSealed tubeInert atmosphere; Reagent/catalystSolvent;
参考文献
Fan, Shilu; Zhang, Xingang; Chen, Zhao
Organic Letters, 2012 , vol. 14, # 18 p. 4950 - 4953,4
95-16-9
苯并噻唑
+
59919-11-8
→
反应条件
4276-60-2
+
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 3 h; Inert atmosphereReflux;
参考文献
Tetrahedron Letters, , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
54394-72-8
→
反应条件
615-22-5
+
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; dimethyl-disulfide; 1,2-bis-(diphenylphosphino)ethane in tetrahydrofuran T=90°C; 3 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
→
反应条件
39544-84-8
+
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
1300105-87-6
→
反应条件
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
59919-17-4
→
反应条件
39544-83-7
+
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
1300105-88-7
→
反应条件
1300105-89-8
+
611-70-1
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene 3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Toriyama, Fumihiko; Yamaguchi, Masahiko
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2344 - 2347
95-16-9
苯并噻唑
+
613-94-5
→
反应条件
1629-75-0
+
93-97-0
反应条件
potassium permanganate; sulfuric acid; acetic acid T=0°C; 0.25 h; Inert atmosphere;
参考文献
Amos, Ruth I. J.; Gourlay, Brendon S.; Yates, Brian F.; Schiesser, Carl H.; Lewis, Trevor W.; Smith, Jason A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 1 p. 170 - 176
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