您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻唑
合成路线
（共 604 条）
95-16-9
苯并噻唑
+
1878-68-8
对溴苯乙酸
→
反应条件
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
oxygen; copper diacetate in dimethyl sulfoxide T=130°C; 26 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
95-16-9
苯并噻唑
+
99-90-1
4-溴苯乙酮
→
反应条件
140935-32-6
+
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h; Overall yield = 73 percent;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
95-16-9
苯并噻唑
+
589-87-7
对溴碘苯
→
反应条件
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
tetrabutylammomium bromide; silver(I) acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=120°C; 18 h; Molecular sieveInert atmosphere;
参考文献
Saha, Debasree; Adak, Laksmikanta; Ranu, Brindaban C.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5624 - 5627
95-16-9
苯并噻唑
+
34176-08-4
→
反应条件
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1,4-dioxane; diethylene glycol dimethyl ether T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
95-16-9
苯并噻唑
+
2039-82-9
4-溴苯乙烯
→
反应条件
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
95-16-9
苯并噻唑
+
7099-87-8
2-(4-溴苯基)-2-氧代乙酸
→
反应条件
19654-19-4
1-(2-苯并噻唑基)-4-溴苯
反应条件
1: in water; dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere; 2: With dipotassium peroxodisulfate 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
95-16-9
苯并噻唑
+
78191-00-1
N-甲氧基-N-甲基乙酰胺
→
反应条件
1629-78-3
2-乙酰苯并噻唑
反应条件
1: cyclobenzothiazole With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: N,O-dimethylacetohydroxamic acid in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
VERTEX PHARMACEUTICALS INCORPORATED
Patent: WO2004/87699 A2, 2004 ;
Location in patent: Page 88-89 ;
WO 2004/087699 A2
95-16-9
苯并噻唑
+
127-19-5
N,N-二甲基乙酰胺
→
反应条件
1629-78-3
2-乙酰苯并噻唑
反应条件
n-butyllithium in tetrahydrofuran; hexane -78 deg C, 1 h; RT, 30 min;
参考文献
Chikashita, Hidenori; Ishibaba, Megumi; Ori, Keiji; Itoh, Kazuyoshi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3637 - 3648
95-16-9
苯并噻唑
+
541-46-8
异戊酰胺
→
反应条件
1629-78-3
2-乙酰苯并噻唑
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 15 min; 2.) THF, allowed to r.t. during 30 min; Yield given. Multistep reaction;
参考文献
Ohta, Shunsaku; Hayakawa, Satoshi; Moriwaki, Hiroki; Harada, Suzumi; Okamoto, Masao
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 12 p. 4916 - 4926
95-16-9
苯并噻唑
+
75-07-0
→
反应条件
1629-78-3
2-乙酰苯并噻唑
反应条件
tert.-butylhydroperoxide; sulfuric acid; iron(II) sulfate
参考文献
Caronna,T. et al.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 1747 - 1750
首页
上一页
1
...
34
35
36
37
38
39
40
...
61
下一页
末页
到第
页
确定
