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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻唑
合成路线
（共 604 条）
95-16-9
苯并噻唑
+
1765-93-1
4-氟苯硼酸
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
anhydrous iron chloride; Cu(OAc)2*2H2O; palladium dichloride in N,N-dimethyl-formamide T=120°C; 24 h;
参考文献
Wu, Xiang-Mei; Shen, Qiu-Xian
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 668 - 673
95-16-9
苯并噻唑
+
459-56-3
对氟苯甲醇
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
95-16-9
苯并噻唑
+
460-00-4
对溴氟苯
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
palladium diacetate; copper (II) acetate monohydrate; potassium carbonate; triphenylphosphine in toluene 6 h; Reflux;
参考文献
Yan, Xue-Ming; Mao, Xue-Rong; Huang, Zhi-Zhen
Heterocycles, 2011 , vol. 83, # 6 p. 1371 - 1376
95-16-9
苯并噻唑
+
352-33-0
1-氯-4-氟苯
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
[Fe(II)(C5H5)(C5H4PPh2)]; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=140°C; 40 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
95-16-9
苯并噻唑
+
32222-45-0
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
oxygen; copper(II) sulfate in dimethyl sulfoxide T=130°C; 22 h; Sealed tube;
参考文献
Song, Qiuling; Feng, Qiang; Zhou, Mingxin
Organic Letters, 2013 , vol. 15, # 23 p. 5990 - 5993
95-16-9
苯并噻唑
+
403-42-9
→
反应条件
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide T=100°C; 12 h; Overall yield = 63 percent;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
95-16-9
苯并噻唑
+
459-57-4
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
iron sulphate heptahydrate; oxygen in diethylene glycol dimethyl ether; water T=150°C; 20 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
95-16-9
苯并噻唑
+
824-80-6
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
palladium diacetate; copper (II) acetate monohydrate in 1-methyl-pyrrolidin-2-one; diethylene glycol dimethyl ether T=120°C; 24 h; sealed vessel;
参考文献
Chen, Ru; Liu, Saiwen; Liu, Xinhua; Yang, Luo; Deng, Guo-Jun
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7675 - 7679
95-16-9
苯并噻唑
+
352-34-1
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; lithium tert-butylate in 1,4-dioxane T=120°C; 36 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
95-16-9
苯并噻唑
+
2251-76-5
→
反应条件
1629-26-1
2-(4-氟苯基)-苯并噻唑
反应条件
1: in water; dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere; 2: With dipotassium peroxodisulfate 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
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