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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯并噻唑
合成路线
（共 604 条）
110-86-1
吡啶
+
95-16-9
苯并噻唑
→
反应条件
716-80-3
2-(2-吡啶)苯并噻唑
反应条件
triethylamine; mercury dichloride; trichlorophosphate Substitution;
参考文献
Komarov, Igor V.; Strizhak, Aleksandr V.; Kornilov, Mikhail Yu.; Zarudnitskiy, Evgeniy; Tolmachev, Andrey A.
Synthetic Communications, 2000 , vol. 30, # 2 p. 243 - 252
694-59-7
吡啶-N-氧化物
+
95-16-9
苯并噻唑
→
反应条件
716-80-3
2-(2-吡啶)苯并噻唑
反应条件
1: caesium carbonate; palladium diacetate; Cu(II) pivalate; copper(I) bromide / 1,4-dioxane; dimethyl sulfoxide / 12 h / 110 °C / |Schlenk technique; |Inert atmosphere 2: phosphorus trichoride / dichloromethane / 5 h / |Reflux View Scheme
参考文献
Fu, Xiao-Pu; Xuan, Qing-Qing; Liu, Li; Wang, Dong; Chen, Yong-Jun; Li, Chao-Jun
Tetrahedron, 2013 , vol. 69, # 22 p. 4436 - 4444
95-16-9
苯并噻唑
+
2033-24-1
米氏酸
+
1087-09-8
二苯甲酰基乙炔
→
反应条件
反应条件
in dichloromethane T=35°C; 120 h; Mechanism;
参考文献
Adib, Mehdi; Sheibani, Esmaeil; Zhu, Long-Guan; Bijanzadeh, Hamid Reza
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4420 - 4422
95-16-9
苯并噻唑
+
70-11-1
2-溴苯乙酮
→
反应条件
7467-00-7
反应条件
T=100 - 120°C; 6 h;
参考文献
Singh, Harjit; Singh, Daman Jit; Kumar, Subodh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 217 - 222
95-16-9
苯并噻唑
→
反应条件
654070-00-5
6-碘苯并[d]噻唑
反应条件
1.1: sulfuric acid; nitric acid / 0 - 20 °C 2.1: hydrogenchloride; iron / ethanol / 0.67 h / Sonication 3.1: sulfuric acid; sodium nitrite / acetic acid / 0.5 h / 20 °C 3.2: 20 - 70 °C View Scheme
参考文献
Hrobarik, Peter; Hrobarikova, Veronika; Sigmundova, Ivica; Zahradnik, Pavol; Fakis, Mihalis; Polyzos, Ioannis; Persephonis, Peter
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8726 - 8736
95-16-9
苯并噻唑
+
99-40-1
→
反应条件
6623-57-0
反应条件
in neat (no solvent) T=100°C; 2 h;
参考文献
Bahner,C.T.; Kinder,H.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1464 - 1465
95-16-9
苯并噻唑
+
111-85-3
→
反应条件
6634-55-5
反应条件
copper(l) iodide; [(diglyme)NiBr2]; diethylene glycol dimethyl ether; sodium iodide; lithium tert-butylate in 1,4-dioxane T=140°C; 16 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Punji, Benudhar; Song, Weifeng
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3325 - 3329
95-16-9
苯并噻唑
+
100-39-0
→
反应条件
67219-33-4
反应条件
1: cyclobenzothiazole With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: With (DABCO)*(SO2)2 in tetrahydrofuran; hexane T=-40°C; 1 h; Inert atmosphere; 3: benzyl bromide in N,N-dimethyl-formamide T=120°C; 3 h; Inert atmosphereMicrowave irradiation;
参考文献
Deeming, Alex S.; Russell, Claire J.; Hennessy, Alan J.; Willis, Michael C.
Organic Letters, 2014 , vol. 16, # 1 p. 150 - 153
95-16-9
苯并噻唑
+
5122-94-1
→
反应条件
67362-98-5
反应条件
potassium phosphate; 1,10-phenanthroline; copper diacetate; palladium diacetate in dimethyl sulfoxide T=80°C; 24 h;
参考文献
Ranjit, Sadananda; Liu, Xiaogang
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1105 - 1108
95-16-9
苯并噻唑
+
127292-60-8
→
反应条件
67362-98-5
反应条件
dipotassium peroxodisulfate; potassium tert-butylate in water; dimethyl sulfoxide T=100°C; 8 h;
参考文献
Yang, Zhiyong; Wang, Anwei; Chen, Xiang; Gui, Qingwen; Liu, Jidan; Tan, Ze; Wang, Hua; Shi, Ji-Cheng
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-W0351-L, p. 1549 - 1554
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