boron trifluoride diethyl etherate in dichloromethane
12 h;
参考文献
Banerji, J.; Saha, M.; Chakrabarti, R.; Das, A. K.; Pandit, U. K.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1204 - 1208
1: n-butyllithium / tetrahydrofuran / 0.08 h / -70 °C
2: tetrahydrofuran / 0.17 h / -70 °C
3: tert-butyllithium / tetrahydrofuran; pentane / 0.75 h / -20 °C
4: 2N sulfuric acid / tetrahydrofuran; pentane; H2O / 3 h / -70 °C
5: 0.02 h / 210 °C
6: n-butyllithium / tetrahydrofuran / 0.08 h / -70 °C
7: tetrahydrofuran / 0.17 h / -70 °C
8: tert-butyllithium / tetrahydrofuran; pentane / 0.75 h / -20 °C
9: 2N sulfuric acid / tetrahydrofuran; pentane; H2O / 3 h / -70 °C
10: 0.02 h / 210 °C
View Scheme
参考文献
Katritzky, Alan R.; Akutagawa, Kunihiko
Journal of the American Chemical Society, 1986 , vol. 108, # 21 p. 6808 - 6809
