boron trifluoride diethyl etherate in dichloromethane

5-sulfo salicylic acid in methanol Heating;

pyridine; chloroform

hydrogenchloride; diethyl ether Zersetzen des entstandenen Ketimid-hydrochlorids mit Wasser und etwas Ammoniak auf dem Wasserbad;

暂无反应条件数据

暂无反应条件数据

1.1: sodium hydride / tetrahydrofuran; hexane / 1 h / 0 °C / |Inert atmosphere; |Reflux 1.2: 0.42 h / 10 - 20 °C / |Inert atmosphere 2.1: AlCl3, aluminium chloride / dichloromethane / 3 h / 0 °C / |Inert atmosphere 3.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 3 h / |Inert atmosphere; |Reflux 4.1: triphenylphosphine / tetrahydrofuran / 6 h / |Inert atmosphere; |Reflux 4.2: 24 h / 20 °C / |Inert atmosphere 5.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere 6.1: N,N-dimethyl-formamide / 3 h / 20 °C / |Inert atmosphere 7.1: potassium carbonate / tetrahydrofuran / 24 h / 20 °C / |Inert atmosphere 7.2: 24 h / |Reflux; |Inert atmosphere 8.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 2 h / |Inert atmosphere; |Reflux 9.1: tetra(n-butyl)ammonium dichromate(VI) / chloroform / 10 h / |Inert atmosphere; |Reflux 10.1: boron tribromide / dichloromethane / 0.08 h / 0 °C / |Inert atmosphere 11.1: iron; calcium chloride / water; ethanol / 5 h / |Inert atmosphere; |Reflux 12.1: sodium hydroxide; oxygen / water; dimethyl sulfoxide / 24 h / 20 °C / |Inert atmosphere View Scheme

1.1: sodium hydride / tetrahydrofuran; hexane / 1 h / 0 °C / |Inert atmosphere; |Reflux 1.2: 0.42 h / 10 - 20 °C / |Inert atmosphere 2.1: AlCl3, aluminium chloride / dichloromethane / 3 h / 0 °C / |Inert atmosphere 3.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 3 h / |Inert atmosphere; |Reflux 4.1: triphenylphosphine / tetrahydrofuran / 6 h / |Inert atmosphere; |Reflux 4.2: 24 h / 20 °C / |Inert atmosphere 5.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere 6.1: N,N-dimethyl-formamide / 3 h / 20 °C / |Inert atmosphere 7.1: potassium carbonate / tetrahydrofuran / 24 h / 20 °C / |Inert atmosphere 7.2: 24 h / |Reflux; |Inert atmosphere 8.1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / 2 h / |Inert atmosphere; |Reflux 9.1: tetra(n-butyl)ammonium dichromate(VI) / chloroform / 10 h / |Inert atmosphere; |Reflux 10.1: boron tribromide / dichloromethane / 0.08 h / 0 °C / |Inert atmosphere 11.1: sodium hydroxide / water; dimethyl sulfoxide / 3 h / 20 °C / |Inert atmosphere 12.1: palladium 10 on activated carbon; hydrogen / ethanol / 6 h / 20 °C 12.2: 1 h / 0 °C / |Inert atmosphere View Scheme

air; cadmium(II) sulphide in water 0.25 h; Irradiation; Mechanism;

in glycerol T=100°C; 15 h;