1: 1-(2-methoxyethoxy)-2-methylbenzene With sec.-butyllithium in diethyl ether T=-30°C; 2 h; 2: methyl iodide With N,N,N',N,-tetramethylethylenediamine in diethyl ether T=-30 - 20°C; Further stages.;
perchloric acid; Fe(ClO4); hexaoxo-.mu.-peroxodisulfate(2-); Cu(II) perchlorate in water; acetonitrile Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 49, # 9 p. 1607 - 1613
