Norris; Turner
Journal of the American Chemical Society, 1939 , vol. 61, p. 2128,2130
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Pajeau; Fierens
Bulletin de la Societe Chimique de France, 1949 , p. 587,588
1: 2,6-dimethylphenyl MgBr With zinc(II) chloride in tetrahydrofuran
T=20°C; 0.333333 h;
2: ortho-chlorotoluene With Pd0(tris(tert-butyl)phosphine)2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi reaction; 18 h; Further stages.;
参考文献
Dai; Fu
Journal of the American Chemical Society, 2001 , vol. 123, # 12 p. 2719 - 2724
1: 1-bromo-2,6-dimethyl-benzene With magnesium in tetrahydrofuran
2: ortho-chlorotoluene With tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran
T=25°C; Kumada-Corriu cross-coupling; 24 h; Further stages.;
参考文献
Wolf, Christian; Xu, Hanhui
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 162 - 167