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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻氯苯酚
合成路线
（共 643 条）
95-57-8
邻氯苯酚
+
108-24-7
乙酸酐
+
108-95-2
苯酚
→
反应条件
102932-05-8
4-溴-2-氯乙酸苯酯
+
1927-95-3
4-溴苯基乙酸酯
+
1829-37-4
1-乙酰氧基-2-溴苯
+
102932-04-7
反应条件
1: 2-chlorophenol; phenol With vanadate(V)-dependent bromoperoxidase I from Ascophyllum nodosum; dihydrogen peroxide; sodium bromide in water; tert-butyl alcohol T=25°C; 24 h; Enzymatic reaction; 2: acetic anhydride With Zn(ClO4)2*6H2O in diethyl ether T=23°C; 16 h; ConcentrationReagent/catalyst;
参考文献
Wischang, Diana; Hartung, Jens
Tetrahedron, 2012 , vol. 68, # 46 p. 9456 - 9463
95-57-8
邻氯苯酚
→
反应条件
2653-89-6
反应条件
1: 34 percent / K2CO3 / dimethylsulfoxide / 24 h / 40 °C 2: 3 percent Chromat. / ethyl p-tert-butyl-benzoate anion; t-BuOH / liquid ammonia / 2 h / Irradiation View Scheme
参考文献
Bardagi, Javier I.; Vaillard, Santiago E.; Rossi, Roberto A.
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3149 - 3152
116-14-3
四氟乙烯
+
95-57-8
邻氯苯酚
→
反应条件
55751-39-8
+
2338-64-9
+
64726-06-3
+
97586-25-9
反应条件
T=620 - 630°C; flow-type copyrolysis; Product distribution;
参考文献
Platonov, V. E.; Malyuta, N. G.; Yakobson, G. G.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 2 p. 345 - 353
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 2 p. 383 - 391
95-57-8
邻氯苯酚
→
反应条件
13524-78-2
反应条件
1.1: potassium carbonate / dimethylformamide 2.1: nBu4N(1+)*BF4(1-) / Ni(cyclam)(2+)*2BF4(1-) / dimethylformamide / 20 °C / 760 Torr / Electrolysis; Mg/Ni electrodes 2.2: 4 percent / K2CO3 / 10 h / 50 °C View Scheme
参考文献
Olivero; Dunach
European Journal of Organic Chemistry, 1999 , # 8 p. 1885 - 1891
95-57-8
邻氯苯酚
→
反应条件
13524-73-7
反应条件
1: 63 percent / sodium hydride / dimethylformamide 2: 48 percent Chromat. / 10-methyl-9,10-dihydroacridine/NaBH4 / dimethylformamide / Irradiation View Scheme
参考文献
Boisvert, Guy; Giasson, Richard
Tetrahedron Letters, 1992 , vol. 33, # 44 p. 6587 - 6590
95-57-8
邻氯苯酚
→
反应条件
15459-49-1
反应条件
sodium periodate; potassium iodide; sodium chloride in water; acetic acid T=25°C; 0.25 h;
参考文献
Emmanuvel, Lourdusamy; Shukla, Ravi Kant; Sudalai, Arumugam; Gurunath, Suryavanshi; Sivaram, Swaminathan
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4793 - 4796
95-57-8
邻氯苯酚
→
反应条件
4526-56-1
+
15459-49-1
+
116130-33-7
+
846040-36-6
反应条件
1: With N-iodo-succinimide; toluene-4-sulfonic acid in acetonitrile T=20°C; 14 h; 2: With N-bromosuccinmide in acetonitrile T=20°C; 4 h;
参考文献
Bovonsombat, Pakorn; Leykajarakul, Juthamard; Khan, Chiraphorn; Pla-on, Kawin; Krause, Michael M.; Khanthapura, Pratheep; Ali, Rameez; Doowa, Niran
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2664 - 2667
95-57-8
邻氯苯酚
→
反应条件
28177-52-8
+
15459-49-1
+
116130-33-7
反应条件
N-iodo-succinimide in acetonitrile T=20°C; 14 h;
参考文献
Bovonsombat, Pakorn; Leykajarakul, Juthamard; Khan, Chiraphorn; Pla-on, Kawin; Krause, Michael M.; Khanthapura, Pratheep; Ali, Rameez; Doowa, Niran
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2664 - 2667
95-57-8
邻氯苯酚
→
反应条件
15459-49-1
反应条件
暂无反应条件数据
参考文献
Kohn; Rabinowitsch
Monatshefte fuer Chemie, 1927 , vol. 48, p. 359
95-57-8
邻氯苯酚
+
13139-86-1
→
反应条件
21849-91-2
反应条件
1: 4-methoxyphenyl magnesium bromide With C24H52Cl2O12P4Pd2 in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada-Corriu cross-coupling reaction; 0.0833333 h; Inert atmosphere; 2: 2-chlorophenol in tetrahydrofuran; 1,4-dioxane T=110°C; Kumada-Corriu cross-coupling reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Fenner, Sabine; Kornhaab, Christoph; Schulzke, Carola
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2965 - 2971
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