暂无反应条件数据

暂无反应条件数据

aluminium trichloride T=-10°C;

T=-10°C;

1: HCl; benzene; AlCl3 / weiteres Reagens: CuCl; Zersetzung des Reaktionsproduktes mit Eis 2: concentrated sulfuric acid; KNO3 / -10 - -5 °C 3: concentrated sulfuric acid; KNO3 View Scheme

CsSO4F in acetonitrile T=35 - 40°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;

beim Bromieren;

sulfur dioxide; bromine; nitric acid

暂无反应条件数据

1: 71 percent / conc. hydrochloric acid 2: 53 percent / 750 °C / 0 Torr 3: 63 percent / 400 °C / 760 Torr 4: 60 percent / stannic chloride / CH2Cl2 / 1.) 0 deg C, 4 h, 2.) room temperature, 2 d 5: 100 percent / sodium borohydride / methanol; benzene / 2 h / Ambient temperature 6: 100 percent / thionyl chloride, pyridine / benzene / 1.) room temperature, 2 h, 2.) reflux, 1 h 7: 40 percent / 700 °C / 0.01 Torr 8: 98 percent / stannic chloride / CH2Cl2 / 1.) 0 deg C, 5 h, 2.) room temperature, 8 h 9: 96 percent / lithium aluminium hydride / diethyl ether / 20 h / Ambient temperature 10: 93 percent / thionyl chloride, pyridine / 1.) room temperature, 21 h, 2.) reflux, 1 h 11: 57 percent / 650 °C / 0.01 Torr 12: 7 percent / lithium, ethylamine, n-propylamine / 10 h / Ambient temperature View Scheme