4-氯-1,2-苯二胺合成路线 (共 167 条)
参考文献
Rao; Ratnam
Proceedings - Indian Academy of Sciences, Section A, 1958 , # 48 p. 256,258, 260
反应条件
1: 66 percent / SeO2 2: 90 percent / NaNO3; aq. H2SO4 / 100 °C 3: 52 percent / aq. HI; aq. HCl View Scheme
参考文献
Keana; Kher; Sui Xiong Cai; Dinsmore; Glenn; Guastella; Huang; Ilyin; Lu; Mouser; Woodward; Weber
Journal of Medicinal Chemistry, 1995 , vol. 38, # 22 p. 4367 - 4379
反应条件
1: 4N HCl / 4 h / Heating 2: 46 percent / CH3ONa / methanol / 4 h / Heating View Scheme
参考文献
Garuti; Ghedini; Leoni; Baraldi; Dionisotti
Farmaco, 1993 , vol. 48, # 11 p. 1531 - 1546
反应条件
[PMIM(SO3H)[OTf]] T=45 - 46°C; 0.166667 h; Ionic liquidSonicationneat (no solvent);
参考文献
Aridoss, Gopalakrishnan; Laali, Kenneth K.
European Journal of Organic Chemistry, 2011 , # 15 p. 2827 - 2835
反应条件
RuCl2(dppe)2; hydrogen T=120°C; P=112511 Torr; 40 h; Green chemistry;
参考文献
Yu, Bo; Zhang, Hongye; Zhao, Yanfei; Chen, Sha; Xu, Jilei; Huang, Changliang; Liu, Zhimin
Green Chemistry, 2013 , vol. 15, # 1 p. 95 - 99
反应条件
tetrabutyl-ammonium chloride in water; toluene T=160°C; 0.25 h; Microwave irradiation;
参考文献
Karuvalam, Ranjith P.; Haridas, Karickal R.; Shetty, Suchetha N.
Journal of the Chilean Chemical Society, 2012 , vol. 57, # 2 p. 1122 - 1125,4
反应条件
hexafluoroisopropyl alcohol T=20°C; 2 h; chemoselective reaction;
参考文献
Khaksar, Samad; Heydari, Akbar; Tajbakhsh, Mahmood; Vahdat, Seyed Mohammad
Journal of Fluorine Chemistry, 2010 , vol. 131, # 12 p. 1377 - 1381
反应条件
in toluene 1.) 2 h, RT, 2.) 2 h, reflux;
参考文献
Stanovnik, Branko; Bajt, OLiver; Balcic, Branko; Koren, Bozidar; Prhavc, Marija; et al.
Heterocycles, 1984 , vol. 22, # 7 p. 1545 - 1554
反应条件
air; silver-loaded TiO2/montmorillonite K10 in acetonitrile 8 h; Solar light irradiation;
参考文献
Selvam, Kaliyamoorthy; Annadhasan, Mari; Velmurugan, Rengasamy; Swaminathan, Meenakshisundaram
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 7 p. 831 - 837
反应条件
air; silver-loaded TiO2/montmorillonite K10 in acetonitrile 8 h; Solar light irradiation;
参考文献
Selvam, Kaliyamoorthy; Annadhasan, Mari; Velmurugan, Rengasamy; Swaminathan, Meenakshisundaram
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 7 p. 831 - 837