1: Jone's reagent / diethyl ether / 38 h / 0 - 20 °C
2: sodium dithionite / diethyl ether; water
3: methanesulfonic acid / 3 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Ciampi, Simone; James, Michael; Le Saux, Guillaume; Gaus, Katharina; Justin Gooding
Journal of the American Chemical Society, 2012 , vol. 134, # 2 p. 844 - 847