1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
T=26.9°C; Zusammensetzung des Gleichgewichtsgemisches;
参考文献
Hastings; Nicholson
Journal of Physical Chemistry, 1957 , vol. 61, p. 730,734
反应条件
chlorosulfonic acid Versetzen mit Eiswasser und Abfiltrieren des gefaellten Durolsulfonsaeurechlorids sowie Bis-<2.3.5.6-tetramethyl-phenyl>-sulfons, Loesen diese in Alkohol, Kuehlen auf 0grad und Umkrystallisation des ausgefaellten Chlorids aus Aether;
参考文献
Huntress; Autenrieth
Journal of the American Chemical Society, 1941 , vol. 63, p. 3446
反应条件
boron trifluoride diethyl etherate; potassium iodide; Tl(OCOCF3)3 1.) trifluoroacetic acid, 1 h, 2.) water, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
McKillop, Alexander; Turrell, Andrew G.; Young, Derek W.; Taylor, Edward C.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6504 - 6512
反应条件
dicloroiodoisocyanuric acid in acetonitrile T=20°C; 3 h; Darkness; regioselective reaction;
参考文献
Journal of the Brazilian Chemical Society, , vol. 23, # 2 p. 228 - 235
反应条件
hydrogenchloride; α,α,α-trifluorotoluene; dihydrogen peroxide; iodine in 2,2,2-trifluoroethanol; water T=20°C; 12 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 7 p. 1243 - 1248
反应条件
iodine cloride; 1,3,5-trimethyl-benzene in various solvent(s) T=20°C; 0.5 h; Kinetics; Further Variations:ReagentsSolvents;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1516 - 1521
反应条件
hydrogen bromide; acetic acid T=120°C; 8 h;
参考文献
Made, A. W. van der; Made, R. H. van der
Journal of Organic Chemistry, 1993 , vol. 58, # 5 p. 1262 - 1263
参考文献
Nightingale; Wadsworth
Journal of the American Chemical Society, 1941 , vol. 63, p. 3514,3516
反应条件
aluminium trichloride
参考文献
Alfa Wassermann S.p.A.
Patent: US5107013 A1, 1992 ;
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane Bromination;
参考文献
Guo, Zhengming; Zheng, Xiaozhang; Thompson, Walter; Dugdale, Marion; Gollamudi, Ram
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 5 p. 1041 - 1058