1,2,4,5-四甲基苯合成路线 （共 381 条）
反应条件
1: |Heating 2: sodium hydrogencarbonate; water / methanol / 40 °C View Scheme
参考文献
Yuan, Changxia; Liang, Yong; Hernandez, Taylor; Berriochoa, Adrian; Houk, Kendall N.; Siegel, Dionicio
Nature, 2013 , vol. 499, # 7457 p. 192 - 196
反应条件
bromine in tetrachloromethane HeatingIrradiation;
参考文献
Shepherd, Michael K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 961 - 970
反应条件
in dichloromethane; acetonitrile -45 deg C to room temperature;
参考文献
Kol, Moshe; Rozen, Shlomo
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1593 - 1595
反应条件
in dichloromethane; acetonitrile -45 deg C to room temperature; other aromatic hydrocarbons; Mechanism;
参考文献
Kol, Moshe; Rozen, Shlomo
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1593 - 1595
反应条件
1.1: sodium chloride; hydrogenchloride / water / 5 h / 120 °C 1.2: 24 h / |Reflux 2.1: acetic acid; potassium acetate / 24 h / 120 °C 3.1: potassium hydroxide / ethanol / 24 h / 90 °C 4.1: chromium(VI) oxide; sulfuric acid / water; acetone / 0 - 20 °C View Scheme
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
titanium tetrachloride in dichloromethane Ambient temperature;
参考文献
Yakubov, Alexander P.; Tsyganov, Dmitry V.; Belen'kii, Leonid I.; Krayushkin, Mikhail M.
Tetrahedron, 1993 , vol. 49, # 16 p. 3397 - 3404
反应条件
titanium tetrachloride in dichloromethane T=0°C;
参考文献
Kingston, Eric E.; Eichholzer, John V.; Lyndon, Paul; MacLeod, John K.; Summons, Roger E.
Organic Mass Spectrometry, 1988 , vol. 23, p. 42 - 47
反应条件
AlCl3, aluminium chloride in nitromethane; dichloromethane T=0°C;
参考文献
ZHANG, Biliang; CUI, Zhiyong
Patent: WO2004/41752 A2, 2004 ;
Location in patent: Page 10 ;
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Mutsuo; Fujiwara, Masahiro; Ando, Hisanori
Journal of Organic Chemistry, 1995 , vol. 60, # 12 p. 3846 - 3850
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Mutsuo; Fujiwara, Masahiro; Ando, Hisanori
Journal of Organic Chemistry, 1995 , vol. 60, # 12 p. 3846 - 3850
