1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
TNM in various solvent(s) T=20°C; 0.5 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
TNM in various solvent(s) T=20°C; 2 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
potassium iodide; Tl(OCOCF3)3 1.) trifluoroacetic acid, 30 min, 2.) H2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
McKillop, Alexander; Turrell, Andrew G.; Young, Derek W.; Taylor, Edward C.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6504 - 6512
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 1.5 h; Further byproducts given;
参考文献
Bosch, E.; Kochi, J. K.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3314 - 3325
反应条件
boron trifluoride diethyl etherate; potassium iodide; Tl(OCOCF3)3 1.) trifluoroacetic acid, 1 h, 2.) water, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
McKillop, Alexander; Turrell, Andrew G.; Young, Derek W.; Taylor, Edward C.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6504 - 6512
反应条件
nitrogen(IV) oxide in dichloromethane T=20°C; 4 h; Irradiationwithout irradiation; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
in various solvent(s) T=20°C; 2 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
sulfuric acid in water; acetic acid T=90°C; 3 h; other solvent, other reagent, reaction time; Product distributionMechanism;
参考文献
Gorodetskaya, T. A.; Kozhevnikov, I. V.; Matveev, K. I.; Sidel'nikov, V. N.; Maksimovskaya, R. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 929 - 935
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1010 - 1017
反应条件
N-fluoropyridinium trifluoromethanesulfonate in acetonitrile T=23°C; 8 h; Irradiationother aromatic donors; charge-transfer photochemistry of aromatic EDA complexes with var. X-pyridinium cations; Product distributionMechanism;
参考文献
Bockman, T. M.; Lee, K. Y.; Kochi, J. K.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 9 p. 1581 - 1594
反应条件
sulfuric acid in water; acetic acid T=90°C; 3 h; Product distributionMechanism;
参考文献
Gorodetskaya, T. A.; Kozhevnikov, I. V.; Matveev, K. I.; Sidel'nikov, V. N.; Maksimovskaya, R. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 929 - 935
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1010 - 1017