1,2,4,5-四甲基苯合成路线 （共 381 条）
参考文献
Schnapauff
Chemische Berichte, 1886 , vol. 19, p. 2510
参考文献
Schnapauff
Chemische Berichte, 1886 , vol. 19, p. 2510
反应条件
1: CAN / dimethylsulfoxide / 40 °C 2: dimethylsulfoxide / Ambient temperature View Scheme
参考文献
Cort, Antonella Dalla; Mandolini, Luigi
Gazzetta Chimica Italiana, 1984 , vol. 114, # 5/6 p. 283 - 284
反应条件
1: aqueous formaldehyde; acetic acid; concentrated aqueous hydrochloric acid 2: acetic acid 3: ethanolic KOH View Scheme
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=25°C; P=760 Torr; 12 h;
参考文献
Yoshino, Yasushi; Hayashi, Yoshiaki; Iwahama, Takahiro; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6810 - 6813
反应条件
oxygen; zirconium (IV) sulphate; anhydrous cobalt diacetate; Manganese (II) acetate; 2,6-dihydroxypyromellitimide in acetic acid T=60 - 70°C; P=6000.6 Torr; 2 h; Product distribution / selectivity;
参考文献
US2011/71314 A1, ;
Page/Page column 13-14 ;
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid T=25°C; P=760 Torr; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 20 p. 6810 - 6813
反应条件
nitrogen(IV) oxide in various solvent(s) T=20°C; 0.5 h; in the dark; Title compound not separated from byproducts;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 11 p. 991 - 1008
反应条件
2-hydroxy-1,3-isoindolinedione; xanthone powder; oxygen; anhydrous tetramethylammonium chloride in acetonitrile T=60°C; P=3750.38 Torr; 3 h; Autoclave;
参考文献
Lu, Tingting; Lu, Ming; Yu, Wang; Liu, Zhongjie
Croatica Chemica Acta, 2012 , vol. 85, # 3 p. 277 - 282
反应条件
water; oxygen; bromide; anhydrous cobalt diacetate; Manganese (II) acetate in acetic acid T=95°C; atmospheric pressure; Further byproducts.;
参考文献
Partenheimer, Walt
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 297 - 306
