1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
in various solvent(s) T=20°C; 20 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
nitric acid in sulfuric acid T=25°C; 0.216667 h; in H2SO4 of different concentration, various time; Product distribution;
参考文献
Manglik, Ajay K.; Moodie, Roy B.; Schofield, Kenneth; Dedeoglu, Erol; Dutly, Andreas; Rys, Paul
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1358 - 1366
反应条件
in various solvent(s) T=20°C; 2 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
in acetonitrile Irradiationvarious reaction conditions; Product distributionMechanism;
参考文献
Masnovi, J. M.; Sankararaman, S.; Kochi, J. K.
Journal of the American Chemical Society, 1989 , vol. 111, # 6 p. 2263 - 2276
反应条件
nitrosyl chloride; trifluoroacetic acid in dichloromethane 120 h; in dark; Product distribution;
参考文献
Makhon'kov, D. I.; Cheprakov, A. V.; Rodkin, M. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 2 p. 211 - 217
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 241 - 248
参考文献
Illuminati; Illuminati
Journal of the American Chemical Society, 1953 , vol. 75, p. 2159
反应条件
nitrosyl chloride; trifluoroacetic acid T=20°C; 4.5 h; other time; Product distributionMechanism;
参考文献
Makhon'kov, D. I.; Cheprakov, A. V.; Rodkin, M. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 2 p. 211 - 217
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 2 p. 241 - 248
反应条件
1: aqueous formaldehyde; acetic acid; concentrated aqueous hydrochloric acid View Scheme
参考文献
Fuson; Sperati
Journal of the American Chemical Society, 1941 , vol. 63, p. 2643
反应条件
1: chloromethylation 2: acetone / 15 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, , vol. 21, # 8 p. 1762 - 1772
反应条件
bromine; iodine in dichloromethane 1.5 h; Reflux;
参考文献
Miller, Glen P.; Kaur, Irvinder
Patent: US2011/130593 A1, 2011 ;
Location in patent: Page/Page column 6 ;