1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
hydrogen bromide; [EtNH3][NO3] in water T=30°C; 3 h; Green chemistry; Reagent/catalyst; regioselective reaction;
参考文献
Podgorsek, Ajda; Stavber, Stojan; Zupan, Marko; Iskra, Jernej
Tetrahedron, 2009 , vol. 65, # 22 p. 4429 - 4439
反应条件
hydrogen bromide; [EtNH3][NO3] in water T=30°C; 3 h; Green chemistry; Reagent/catalyst; regioselective reaction;
参考文献
Organic Letters, , vol. 15, # 9 p. 2108 - 2111
反应条件
N-bromosuccinmide; toluene-4-sulfonic acid in methanol 21 h; Ambient temperaturevariation of conditions, other catalysts and reagents, without catalyst, + succinimide (NHS); other polyalkylbenzenes; Product distributionMechanism;
参考文献
Bovonsombat; McNelis
Synthesis, 1993 , # 2 p. 237 - 241
反应条件
1: With hydrogenchloride; sodium chloride in water T=120°C; 5 h; 2: With zinc(II) chloride in water 24 h; Reflux;
参考文献
Hijazi, Akram; Kemmegne-Mbouguen, Justin Claude; Floquet, Sebastien; Marrot, Jerome; Fize, Jennifer; Artero, Vincent; David, Olivier; Magnier, Emmanuel; Pegot, Bruce; Cadot, Emmanuel
Dalton Transactions, 2013 , vol. 42, # 14 p. 4848 - 4858
反应条件
hydrogenchloride; formaldehyd; acetic acid
参考文献
Rhoad; Flory
Journal of the American Chemical Society, 1950 , vol. 72, p. 2216,2219
Full Text Show Details
Aitken et al.
Journal of the Chemical Society, 1950 , p. 331,334
反应条件
acetic anhydride; zinc(II) chloride
参考文献
Esso Research and Eng. Co.
Patent: US2873299 , 1954 ;
参考文献
Rudenko, A. P.; Zarubin, M. Ya.; Fedorova, E. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1609 - 1618
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1762 - 1772
反应条件
N-bromosuccinmide in chloroform Heating;
参考文献
Wu, An-Tai; Liu, Wen-Dar; Chung, Wen-Sheng
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 1 p. 77 - 82
反应条件
aluminium trichloride in chloroform T=25°C; 1 h;
参考文献
Andreou et al.
Tetrahedron, 1980 , vol. 36, p. 2101
反应条件
aluminium trichloride in various solvent(s) T=100°C; 6 h;
参考文献
Journal of Organic Chemistry, , vol. 49, # 20 p. 3832 - 3834