1,2,4,5-四甲基苯合成路线 (共 381 条)
反应条件
aluminium trichloride in tetrachloromethane 1.) 5 deg C, 1 h; 2.) 25 deg C, 1 h;
参考文献
Tetrahedron, , vol. 36, p. 2101
反应条件
carbon disulfide; aluminium trichloride
参考文献
Gray; Walker; Fuson
Journal of the American Chemical Society, 1931 , vol. 53, p. 3494,3496
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Smith; Guss
Journal of the American Chemical Society, 1937 , vol. 59, p. 804
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Kadesch; Weller
Journal of the American Chemical Society, 1941 , vol. 63, p. 1310,1312
反应条件
aluminium trichloride in carbon disulfide T=50°C; 1 h;
参考文献
Tetrahedron, , vol. 36, p. 2101
反应条件
aluminium trichloride in carbon disulfide 1.) 25 deg C, 1 h; 2.) 50 deg C, 3 h;
参考文献
Tetrahedron, , vol. 36, p. 2101
反应条件
in nitromethane cooling;
参考文献
Davlieva; Lindeman; Neretin; Kochi
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 4013 - 4021
反应条件
aluminium trichloride in carbon disulfide T=25°C; 1 h; other acetylation agent, other solvents, other conditions, further tetramethylbenzenes; Product distribution;
参考文献
Andreou et al.
Tetrahedron, 1980 , vol. 36, p. 2101
反应条件
in dichloromethane T=-50°C; 4 h; Irradiationfurther solvents, temperatures; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Fulton, Karen L.; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1996 , vol. 50, # 11 p. 991 - 1008
反应条件
1: dibenzoyl peroxide; tetrachloromethane; N-bromo-succinimide 2: acetic acid 3: ethanolic KOH View Scheme
参考文献
Ried; Bodem
Chemische Berichte, 1956 , vol. 89, p. 2328,2330
反应条件
1: With bromine in tetrachloromethane
T=54°C; Darkness;
2: With bromine in tetrachloromethane
IrradiationReflux;
参考文献
Guo, Xugang; Watson, Mark D.
Macromolecules, 2011 , vol. 44, # 17 p. 6711 - 6716
反应条件
sulfuric acid
T=100°C;
参考文献
Jacobsen
Chemische Berichte, 1886 , vol. 19, p. 1212
Chemische Berichte, 1887 , vol. 20, p. 902