1,2,4,5-四氯苯合成路线 （共 206 条）
反应条件
1: 2-methylpropane-2-thiol With sodium in N,N-dimethyl-formamide T=20°C; 8 h; 2: 1,2,4,5-TeCB in N,N-dimethyl-formamide 3 h; Heating;
参考文献
Xia, Shijing; Villamena, Frederick A.; Hadad, Christopher M.; Kuppusamy, Periannan; Li, Yunbo; Zhu, Hong; Zweier, Jay L.
Journal of Organic Chemistry, 2006 , vol. 71, # 19 p. 7268 - 7279
反应条件
in N,N-dimethyl-formamide T=20°C; Reflux;
参考文献
Rogozhnikova, Olga Yu.; Vasiliev, Vladimir G.; Troitskaya, Tatiana I.; Trukhin, Dmitry V.; Mikhalina, Tatiana V.; Halpern, Howard J.; Tormyshev, Victor M.
European Journal of Organic Chemistry, 2013 , # 16 p. 3347 - 3355
反应条件
isopentyl nitrite Cadogan modification of Gomberg-Bachman;
参考文献
Bolgar; et al.
Chemosphere, 1995 , vol. 31, # 2 p. 2687 - 2705
反应条件
chlorosulfonic acid T=165°C;
参考文献
Chivers,G.E. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 1573 - 1582
反应条件
sulfuric acid; nitric acid T=100°C;
参考文献
Berckmans; Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1925 , vol. 44, p. 852
参考文献
Berckmans; Holleman
Recueil des Travaux Chimiques des Pays-Bas, 1925 , vol. 44, p. 852
反应条件
aluminium trichloride 22 h; Heating;
参考文献
Castaner, J.; Riera, J.
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5445 - 5448
反应条件
sodium isopropylthiolate; sodium 1.) HMPA, 2.) 100 deg C; Yield given. Multistep reaction;
参考文献
Dirk, C. W.; Cox, S. D.; Wellman, D. E.; Wudl, F.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2395 - 2397
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.92 h; Yields of byproduct given;
参考文献
Marques, Carlos Alberto; Selva, Maurizio; Tundo, Pietro
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5256 - 5260
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.5 h; Aliquat 336 and other phase-transfer catalysts, different multiphase systems, different time and solvents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5256 - 5260
