1,2,4,5-四氯苯合成路线 (共 206 条)
反应条件
pyridine; [(FeCp)2(1,2,3,4,5,6,7,8,9-nanomethylfluorene)H][PF6]2 in diethylene glycol dimethyl ether T=125°C; Product distribution; Further Variations:reaction times;
参考文献
Fletcher, Andrew E. D.; Moss, James; Cowley, Andrew R.; O'Hare, Dermot
Chemical Communications, 2007 , # 28 p. 2971 - 2973
反应条件
1: NaAlH2(OCH2CH2OCH3)2 / toluene / 70 °C / relative reactivity in dehalogenation; reaction order 2: NaAlH2(OCH2CH2OCH3)2 / toluene / 70 °C / relative reactivity in dehalogenation View Scheme
参考文献
Trukhin; Adonin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 8 p. 1227 - 1228
反应条件
isopentyl nitrite Cadogan modification of Gomberg-Bachman;
参考文献
Bolgar; et al.
Chemosphere, 1995 , vol. 31, # 2 p. 2687 - 2705
反应条件
isopentyl nitrite T=130°C;
参考文献
Russian Journal of General Chemistry, , vol. 82, # 1 p. 138 - 143
反应条件
dicobalt octacarbonyl in methanol T=65°C; 96 h; P(CO): 2 kg/cm-2;
参考文献
Kazimura, Tsugunori; Kudo, Kiyoshi; Mori, Sadayuki; Sugita, Nobuyuki
Chemistry Letters, 1986 , p. 851 - 854
反应条件
in N,N-dimethyl-formamide T=100°C; 1 h;
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Synthesis, 1983 , # 9 p. 751 - 755
反应条件
sodium in ethanol; N,N-dimethyl-formamide 2.) 100 deg C, 30 min;
参考文献
Bock, Hans; Rauschenbach, Andreas; Naether, Christian; Kleine, Markus; Havlas, Zdenek
Liebigs Annales, 1996 , # 12 p. 2185 - 2194
反应条件
in acetonitrile 25 h; Irradiation; Product distribution;
参考文献
Chemistry Letters, , p. 1589 - 1592
反应条件
in acetonitrile 8 h; Irradiationother polyhalonobenzenes; var. solvents; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 11 p. 2926 - 2933
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.00277778 h; Ambient temperatureother reaction times; other solvent: DMF; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4660 - 4666