1,2,4,5-四氯苯合成路线 （共 206 条）
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.92 h; Yields of byproduct given;
参考文献
Marques, Carlos Alberto; Selva, Maurizio; Tundo, Pietro
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5256 - 5260
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.5 h; Aliquat 336 and other phase-transfer catalysts, different multiphase systems, different time and solvents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5256 - 5260
反应条件
carbon dioxide; tetrabutylammomium bromide in N,N-dimethyl-formamide T=-5 - 0°C; Dehalogenation; Electrochemical reaction; Further byproducts given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 862 - 880
反应条件
pyridine; [(FeCp)2(1,2,3,4,5,6,7,8,9-nanomethylfluorene)H][PF6]2 in diethylene glycol dimethyl ether T=125°C; Product distribution; Further Variations:reaction times;
参考文献
Fletcher, Andrew E. D.; Moss, James; Cowley, Andrew R.; O'Hare, Dermot
Chemical Communications, 2007 , # 28 p. 2971 - 2973
反应条件
1: NaAlH2(OCH2CH2OCH3)2 / toluene / 70 °C / relative reactivity in dehalogenation; reaction order 2: NaAlH2(OCH2CH2OCH3)2 / toluene / 70 °C / relative reactivity in dehalogenation View Scheme
参考文献
Trukhin; Adonin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 8 p. 1227 - 1228
反应条件
in acetonitrile 8 h; Irradiationother polyhalonobenzenes; var. solvents; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 11 p. 2926 - 2933
反应条件
sulfuric acid; sulfur trioxide
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 39, # 6 p. 1596 - 1600
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.00277778 h; Ambient temperatureother reaction times; other solvent: DMF; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4660 - 4666
反应条件
potassium hydroxide; (Tricyclohexyl-n-dodecyl)phosphonium bromide in toluene T=25°C; 2 h;
参考文献
Brunelle, D. J.
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1309 - 1311
反应条件
copper(l) iodide; 1,10-phenanthroline; lithium tert-butylate in N,N'-dimethyl-N,N'-propyleneurea T=125°C; 12 h; Inert atmosphere;
参考文献
Do, Hien-Quang; Khan, Rana M. Kashif; Daugulis, Olafs
Journal of the American Chemical Society, 2008 , vol. 130, # 45 p. 15185 - 15192
