1,2,4,5-四氯苯合成路线 （共 206 条）
反应条件
1: With 1-[2-(diphenylphosphino)phenyl]ethanol; bis(acetylacetonate)nickel(II) in diethyl ether T=45°C; 96 h; 2: With methanol in diethyl ether Product distribution / selectivity;
参考文献
THE UNIVERSITY OF TOKYO
Patent: WO2006/85628 A1, 2006 ;
Location in patent: Page/Page column 34-35 ;
反应条件
in diethyl ether 1.) RT, 24 h, 2.) reflux, 1 h;
参考文献
Saednya, Akbar; Hart, Harold
Synthesis, 1996 , # 12 p. 1455 - 1458
反应条件
sulfuric acid; iodine
参考文献
Istrati
Bulet., vol. 1, p. 156
反应条件
1: 87 percent / AlCl3 / Heating 2: 60 percent / FeSO4, conc. H2SO4 / Heating View Scheme
参考文献
Belen'kii; Gromova; Lichitskii; Krayushkin
Russian Chemical Bulletin, 1997 , vol. 46, # 1 p. 101 - 104
反应条件
potassium hydroxide; hydrogen; palladium on activated charcoal in water T=50°C; 0.5 h; Aliquat 336 and other phase-transfer catalysts, different multiphase systems, different time and solvents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5256 - 5260
反应条件
potassium methanolate; bis(dibenzylideneacetone)-palladium(0) in methanol; toluene T=95°C; Suzuki coupling;
参考文献
Russian Chemical Bulletin, , vol. 56, # 7 p. 1467 - 1469
反应条件
sodium tetrahydroborate; bis(cyclopentadienyl)titanium dichloride in N,N-dimethyl acetamide T=85°C;
参考文献
Liu, Yumin; Schwartz, Jeffrey
Tetrahedron, 1995 , vol. 51, # 15 p. 4471 - 4482
反应条件
carbon dioxide; tetrabutylammomium bromide in N,N-dimethyl-formamide T=-5 - 0°C; Dehalogenation; Electrochemical reaction; Further byproducts given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 6 p. 862 - 880
反应条件
pyridine; [(FeCp)2(1,2,3,4,5,6,7,8,9-nanomethylfluorene)H][PF6]2 in diethylene glycol dimethyl ether T=125°C; Product distribution; Further Variations:reaction times;
参考文献
Fletcher, Andrew E. D.; Moss, James; Cowley, Andrew R.; O'Hare, Dermot
Chemical Communications, 2007 , # 28 p. 2971 - 2973
反应条件
bis(cyclopentadienyl)titanium dichloride; sodium tetrahydroborate; N,N-dimethyl-formamide 1.) 95 deg C, 2.) 52 deg C, 18.5 h; Yield given. Yields of byproduct given;
参考文献
Liu, Yumin; Schwartz, Jeffrey
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 5005 - 5007
