1,2,4,5-四氯苯合成路线 (共 206 条)
反应条件
sodium tetrahydroborate; bis(cyclopentadienyl)titanium dichloride T=95°C; effect of Cp2TiCl2 concentration on induction period of reduction; Rate constant;
参考文献
Liu, Yumin; Schwartz, Jeffrey
Tetrahedron, 1995 , vol. 51, # 15 p. 4471 - 4482
反应条件
T=25°C; 40 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3122 - 3126
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 0.00277778 h; Ambient temperatureother reaction times; other solvent: DMF; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4660 - 4666
反应条件
in acetonitrile 25 h; Irradiation; Product distribution;
参考文献
Chemistry Letters, , p. 1589 - 1592
反应条件
in acetonitrile 8 h; Irradiationother polyhalonobenzenes; var. solvents; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 11 p. 2926 - 2933
反应条件
potassium hydroxide; tetra-(n-butyl)-phosphonium bromide in toluene T=25°C; 2 h;
参考文献
Brunelle, D. J.
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1309 - 1311
反应条件
aluminum tri-bromide; bromine 3 h; Heating;
参考文献
Golounin, A. V.; Shukhta, T. K.; Kirienko, E. K.; Petrova, M. P.; Esavkin, E. V.
Russian Journal of Applied Chemistry, 1994 , vol. 67, # 8.2 p. 1167 - 1169
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1994 , vol. 67, # 8 p. 1324 - 1327
反应条件
1,3-dimethyl-imidazolidin-2-one; magnesium; copper(l) chloride; lithium chloride T=55°C; 17 h;
参考文献
Kitamura, Tsugio; Gondo, Keisuke; Katagiri, Toshimasa
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3421 - 3424
反应条件
potassium phosphate; tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=80°C; 24 h;
参考文献
Burukin; Vasil'ev; Chizhov; Zlotin
Russian Chemical Bulletin, 2005 , vol. 54, # 4 p. 970 - 974
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane 0.333333 h; cooling; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=20°C; 0.333333 h; 3: 1,2,4,5-TeCB With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane Negishi coupling; 24 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 54, # 4 p. 970 - 974