1,2,4,5-四氯苯合成路线 (共 206 条)
反应条件
chlorine; iron(III) chloride
参考文献
Chem. Prumysl.Chem.Abstr., , vol. 8, p. 11
Chem. Prumysl.Chem.Abstr., , p. 19928
US2843637 , ;
US2805264 , ;
反应条件
SbF5 T=0°C; Substitution; 0.5 h; Further byproducts given;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 11 p. 1573 - 1578
参考文献
Justus Liebigs Annalen der Chemie, , vol. 152, p. 238
反应条件
hydrogenchloride; acetic acid anschliessendes Behandeln mit wss. Natriumnitrit-Loesung und mit einer Loesung von Kupfer(I)-chlorid in wss. Salzsaeure;
参考文献
Journal of Scientific and Industrial Research, , vol. 10 B, p. 140,143
反应条件
antimony(V) pentachloride Destillation der auftretenden Aldehyde;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 296, p. 71
Chemische Berichte, , vol. 29, p. 876
反应条件
in ethanol 24 h; Heating; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 48, # 5 p. 727 - 731
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=20 - 40°C; relative reactivity in dehalogenation; Rate constantMechanism;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 59, # 6 p. 1368 - 1383
反应条件
iodine; magnesium; ethylene dibromide 1.) THF, from 10 deg C to 15 deg C, 1 h, 2.) THF, benzene, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 225, # 1 p. 25 - 30
反应条件
hydrogenchloride; copper (I) cyanide Diazotization;
参考文献
Journal of the Chemical Society, , p. 796,801
反应条件
air; N-hexadecyl-N,N,N-trimethylammonium bromide in acetonitrile T=50°C; 0.0333333 h; Irradiationor in acetonitrile/ H2O; in presence of KBr or of Et3N/ KBr or of Et3N; or at other times; Product distributionQuantum yieldMechanism;
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2846 - 2850