二螺[5,1,5,1]十四烷-7,14-二酮合成路线 （共 19 条）
反应条件
phosphorus pentachloride in tetrachloromethane 4 h;
参考文献
Strelow, Thomas; Voss, Juergen; Adiwidjaja, Gunadi
Journal of Chemical Research, Miniprint, 1989 , # 5 p. 1148 - 1161
反应条件
phosphorus pentachloride in tetrachloromethane 4 h; Heating;
参考文献
Komendantov, M. I.; Koptelov, Yu. V.; Kostikov, R. R.; Molchanov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 889 - 892
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 986 - 990
反应条件
hydrogenchloride; hydrogen sulfide; zinc(II) chloride in methanol; ethanol
参考文献
Freund, Wolfgang; Huenig, Siegfried
Journal of Organic Chemistry, 1987 , vol. 52, # 11 p. 2154 - 2161
反应条件
1: 70 percent / P2S5 / pyridine / 2 h / Heating 2: 45 percent / P2S5 / pyridine / 2 h / Heating View Scheme
参考文献
Muthuramu, K.; Sundari, B.; Ramamurthy, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4482 - 4487
反应条件
tetraphosphorus decasulfide in pyridine 2 h; Heating;
参考文献
Sundari, B.; Ramamurthy, V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 498 - 501
Title/Abstract Full Text Show Details
Muthuramu, K.; Sundari, B.; Ramamurthy, V.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4482 - 4487
反应条件
hydrogenchloride; hydrogen sulfide; zinc(II) chloride in methanol; ethanol
参考文献
Journal of Organic Chemistry, , vol. 52, # 11 p. 2154 - 2161
反应条件
triethylamine in diethyl ether
T=0 - 20°C; Inert atmosphere;
参考文献
Kuzmanich, Gregory; Garcia-Garibay, Miguel A.
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 10 p. 883 - 888
反应条件
1: 66 percent / Zn / tetrahydrofuran / 0.5 h / 20 °C
2: 2.) Et3N / 1.) THF, hexane, -78 deg C, 0,5 h, 2.) 25 deg, 2 h
View Scheme
参考文献
Baigrie, Lynn M.; Lenoir, Dieter; Seikaly, Hani R.; Tidwell, Thomas T.
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2105 - 2109
反应条件
T=190 - 210°C; P=0.1 - 0.2 Torr; 0.25 h;
参考文献
Letcher, Roy M.; Choi, Michael C.K.; Acheson, R.Morrin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 3 p. 515 - 526
反应条件
in 1,3,5-trimethyl-benzene
T=150°C;
参考文献
Regitz,M.; Rueter,J.
Chemische Berichte, 1969 , vol. 102, p. 3877 - 3890
