3,4-二氢-2,2,5,7,8-五甲基-2H-1-苯并吡喃-6-酚合成路线 （共 40 条）
反应条件
1: aluminium chloride; nitrobenzene
2: methanol; amalgamated zinc; aqueous HCl / unter Einleiten von Chlorwasserstoff
View Scheme
参考文献
John et al.
Chemische Berichte, 1938 , vol. 71, p. 2637,2647
反应条件
tin(IV) chloride in chloroform
T=60°C; 15 h; variation of acid, solvent, temperature, time; Product distribution;
参考文献
Julia, Marc; Nel, Maurice; Uguen, Daniel
Bulletin de la Societe Chimique de France, 1987 , # 3 p. 487 - 492
反应条件
acetic acid; zinc(II) chloride
参考文献
Smith et al.
Journal of Organic Chemistry, 1939 , vol. 4, p. 340
参考文献
Smith et al.
Journal of Organic Chemistry, 1939 , vol. 4, p. 340
反应条件
in acetonitrile
T=24.84°C; Kinetics;
参考文献
Nakanishi, Ikuo; Fukuhara, Kiyoshi; Shimada, Tomokazu; Ohkubo, Kei; Iizuka, Yuko; Inami, Keiko; Mochizuki, Masataka; Urano, Shiro; Itoh, Shinobu; Miyata, Naoki; Fukuzumi, Shunichi
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 9 p. 1520 - 1524
反应条件
hydrogenchloride; potassium hydroxide; iodine
1.) methanol, room temp.; 60 deg C, 1h, 2.) 60 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Burton, G. W.; Doba, T.; Gabe, E. J.; Hughes, L.; Lee, F. L.; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7053 - 7065
反应条件
potassium hydroxide; iodine
T=50°C; 0.666667 h; Yield given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1987 - 1990
反应条件
triethylamine in dichloromethane
参考文献
Rosenau, Thomas; Adelwoehrer, Christian; Hofinger, Andreas; Mereiter, Kurt; Kosma, Paul
European Journal of Organic Chemistry, 2004 , # 6 p. 1323 - 1329
反应条件
pyridine
T=20°C; 6 h;
参考文献
Patel, Anjan; Netscher, Thomas; Gille, Lars; Mereiter, Kurt; Rosenau, Thomas
Tetrahedron, 2007 , vol. 63, # 24 p. 5312 - 5318
反应条件
potassium carbonate in acetonitrile
T=20°C;
参考文献
Thomas, Joshua D.; Sloan, Kenneth B.
Synthesis, 2008 , # 2 p. 272 - 278
