N-甲氧基-N-甲基-2-呋喃甲酰胺合成路线 (共 13 条)
反应条件
Yield given. Multistep reaction;
参考文献
Basha, Fatima Z.; DeBernardis, John F.
Tetrahedron Letters, 1984 , vol. 25, # 46 p. 5271 - 5274
反应条件
in tetrahydrofuran T=20°C; Grignard reaction; 1 h; Inert atmosphere;
参考文献
Franchi, Luigi; Rinaldi, Marta; Vignaroli, Giulia; Innitzer, Anna; Radi, Marco; Botta, Maurizio
Synthesis, 2010 , # 22 art. no. Z19310SS, p. 3927 - 3933
反应条件
1: 1-bromo undecane With magnesium in diethyl ether
1 h; Heating / reflux;
2: N-methoxy-N-methyl-2-pyrrolecarboxamide in diethyl ether
T=0°C; 3 h;
3: With hydrogenchloride in diethyl ether; water
T=0°C;
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US7161015 B1, 2007 ;
Location in patent: Page/Page column 5 ;