噻蒽 5,10-二氧化物合成路线 (共 16 条)
反应条件
1: ligroine; aluminium chloride / Zersetzen der Reaktionsprodukte mit Wasser
2: nitric acid
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参考文献
Deuss
Recueil des Travaux Chimiques des Pays-Bas, 1908 , vol. 27, p. 147
反应条件
1: aluminium chloride; sulfur / Zersetzen des Reaktionsprodukts mit Wasser
2: chromic acid; glacial acetic acid
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参考文献
Friedel; Crafts
Annales de Chimie (Cachan, France), 1888 , vol. <6> 14, p. 446
反应条件
benzyltriethylammonium permanganate in dichloromethane
other oxidizing agents; Mechanism;
参考文献
May; Yee; Lee
Canadian Journal of Chemistry, 1994 , vol. 72, # 11 p. 2249 - 2254
反应条件
in acetonitrile
72 h; also in the presence of 2,6-di-tert-butyl-4-methylpyridine; also with 18O-labeled oxime; Product distributionMechanism;
参考文献
Chiou, Shishue; Hoque, A. K. M. M.; Shine, Henry J.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3227 - 3232
反应条件
in acetonitrile
also in the presence of 2,6-di-tert-butyl-4-methylpyridine; Product distributionMechanism;
参考文献
Chiou, Shishue; Hoque, A. K. M. M.; Shine, Henry J.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3227 - 3232
反应条件
molybdenum peroxide hexamethylphosphorylamide
speed of oxidation, competitiv by SOSO2;
参考文献
Adam, Waldemar; Lohray, B. Bhushan
Angewandte Chemie, 1986 , vol. 98, # 2 p. 185 - 186