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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2'-脱氧尿苷
合成路线
（共 165 条）
951-78-0
2'-脱氧尿苷
+
292638-85-8
丙烯酸甲酯
→
反应条件
86163-17-9
E-5-(2-羰基甲氧基乙烯基)-2’-脱氧尿苷
反应条件
palladium diacetate in acetonitrile 32 h; Heating;
参考文献
Hirota, Kosaku; Isobe, Yoshiaki; Kitade, Yukio; Maki, Yoshifumi
Synthesis, 1987 , # 5 p. 495 - 496
951-78-0
2'-脱氧尿苷
→
反应条件
61135-33-9
5-乙炔-2-脱氧尿苷
反应条件
1: pyridine / 20 °C 2: ammonium cerium (IV) nitrate; iodine / acetonitrile / 1 h / 80 °C 3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / dichloromethane / 20 h 4: ammonia; water / 2 h 5: methanol; potassium carbonate View Scheme
参考文献
Science China Chemistry, , vol. 54, # 11 p. 1702 - 1710
1664-98-8
甲醛-d2
+
951-78-0
2'-脱氧尿苷
→
反应条件
74848-84-3
胸苷-d3
反应条件
Yield given. Multistep reaction;
参考文献
Shaw, Anthony A.; Cadet, Jean
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 12 p. 2063 - 2070
2314-97-8
三氟碘甲烷
+
951-78-0
2'-脱氧尿苷
→
反应条件
70-00-8
三氟胸苷
反应条件
Fe2(S04)3; sulfuric acid; dihydrogen peroxide in water; dimethyl sulfoxide T=40 - 50°C; 0.333333 h;
参考文献
Tosoh Corporation; Tosoh F- Tech Inc.; SAGAMI CHEMICAL RESEARCH CENTER
Patent: EP1947092 A1, 2008 ;
Location in patent: Page/Page column 43-44 ;
887144-94-7
1-三氟甲基-1,2-苯碘酰-3(H)-酮
+
951-78-0
2'-脱氧尿苷
→
反应条件
70-00-8
三氟胸苷
反应条件
copper(l) iodide in N,N-dimethyl-formamide T=80°C; 23 h; Inert atmosphereSealed tube; regioselective reaction;
参考文献
Fang, Zhongxue; Ning, Yongquan; Mi, Pengbing; Liao, Peiqiu; Bi, Xihe
Organic Letters, 2014 , vol. 16, # 5 p. 1522 - 1525
951-78-0
2'-脱氧尿苷
+
54-20-6
5-三氟甲基尿嘧啶
→
反应条件
70-00-8
三氟胸苷
+
66-22-8
尿嘧啶
反应条件
pyrimidine nucleoside phosphorylase from Bacillus subtilis (E.C. 2.4.2.3) immobilized on Sepabeads EC-EP® in aq. phosphate buffer T=20°C; pH=7.5; 10 h; Enzymatic reaction; Reagent/catalyst;
参考文献
Serra, Immacolata; Bavaro, Teodora; Cecchini, Davide A.; Daly, Simona; Albertini, Alessandra M.; Terreni, Marco; Ubiali, Daniela
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 95, p. 16 - 22
951-78-0
2'-脱氧尿苷
+
69304-49-0
(E)-5-(2-溴乙烯基)尿嘧啶
→
反应条件
66-22-8
尿嘧啶
+
69304-47-8
溴夫定
反应条件
potassium carbonate in aq. phosphate buffer T=20°C; pH=10; 3 h; Enzymatic reaction; Reagent/catalyst;
参考文献
Serra, Immacolata; Bavaro, Teodora; Cecchini, Davide A.; Daly, Simona; Albertini, Alessandra M.; Terreni, Marco; Ubiali, Daniela
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 95, p. 16 - 22
951-78-0
2'-脱氧尿苷
→
反应条件
59-14-3
溴脲苷
反应条件
[MoeMIm][TFA]; N-bromosuccinmide T=25°C; 0.0833333 h;
参考文献
Kumar, Vineet; Yap, Jeremy; Muroyama, Andrew; Malhotra, Sanjay V.
Synthesis, 2009 , # 23 art. no. M01709SS, p. 3957 - 3962
51-20-7
5-溴尿嘧啶
+
951-78-0
2'-脱氧尿苷
→
反应条件
59-14-3
溴脲苷
+
66-22-8
尿嘧啶
反应条件
thymidine phosphorylase from Escherichia coli (E.C. 2.4.2.4) immobilized on Sepabeads EC-EP® in aq. phosphate buffer T=20°C; pH=7.5; 3 h; Enzymatic reaction; Reagent/catalyst;
参考文献
Serra, Immacolata; Bavaro, Teodora; Cecchini, Davide A.; Daly, Simona; Albertini, Alessandra M.; Terreni, Marco; Ubiali, Daniela
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 95, p. 16 - 22
951-78-0
2'-脱氧尿苷
→
反应条件
132101-33-8
1-[(2R,4S,5R)-4-叠氮基-5-(异氰基甲基)四氢呋喃-2-基]嘧啶-2,4-二酮
反应条件
1: 80 percent / triphenylphosphine, HN3, diethyl azodicarboxylate / dimethylformamide; toluene / 2 h / 40 °C 2: 63 percent / triphenylphosphine, diethyl azodicarboxylate / toluene; dioxane / 4 h / 60 °C 3: 72 percent / triphenylphosphine / dimethylformamide; toluene / 4 h / 60 °C 4: 48 percent / LiN3, benzoic acid, / dimethylformamide / 4 h / 130 °C 5: 62 percent / tosyl chloride / pyridine / 16 h / 20 °C View Scheme
参考文献
Hiebl, Johann; Zbiral, Erich; Balzarini, Jan; Clercq, Erik De
Journal of Medicinal Chemistry, 1991 , vol. 34, # 4 p. 1426 - 1430
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