(2,6-二氯甲氧基苯氧基)乙酸合成路线 (共 6 条)
反应条件
sodium hydroxide in water 14 h; Heating;
参考文献
Unge, Sverker von; Lundquist, Knut; Stomberg, Rolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 7 p. 469 - 474
反应条件
lithium hydroxide in tetrahydrofuran
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 8 p. 1185 - 1187
反应条件
1: NaH 2: aq. LiOH / tetrahydrofuran View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 8 p. 1185 - 1187
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane 0 deg C, 2 h -> room temperature; Yields of byproduct given;
参考文献
Unge, Sverker von; Lundquist, Knut; Stomberg, Rolf
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 7 p. 469 - 474
反应条件
sulfuric acid in benzene
参考文献
Czerwinska,E. et al.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1967 , vol. 15, p. 71 - 75
反应条件
1: 83 percent / ethyl chlorocarbonate, Et3N / CHCl3 / Ambient temperature
2: 63 percent / BH3*CH3SCH3 / bis-(2-methoxy-ethyl) ether / 8 h / 80 °C
View Scheme
参考文献
Giardina; Angeli; Brasili; et al.
European Journal of Medicinal Chemistry, 1984 , vol. 19, # 5 p. 411 - 414