反应条件
1.1: hydrogenchloride / 1,4-dioxane / 16 h / 0 - 22 °C / |Inert atmosphere
2.1: sodium methylate / 1,4-dioxane; methanol / 5 - 15 °C / |Inert atmosphere
2.2: 2 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Frutos, Rogelio P.; Wei, Xudong; Patel, Nitinchandra D.; Tampone, Thomas G.; Mulder, Jason A.; Busacca, Carl A.; Senanayake, Chris H.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5800 - 5803
