反应条件
1: 89 percent / CeCl3, n-BuLi / tetrahydrofuran / 2 h / -78 °C
2: 71 percent / NaOEt / ethanol / 0.83 h / Ambient temperature
3: 85 percent / KOH / ethanol; H2O / 1 h / Heating
4: 99 percent / (trimethylsilyl)ethoxyacetylene
5: 66 percent / NaH / tetrahydrofuran / 2 h / Ambient temperature
6: 88 percent / HgO(yellow), 20percent H2SO4 / tetrahydrofuran / 5 h / Heating
View Scheme
参考文献
Tamura; Akai; Kishimoto; Sasho; Kirihara; Kita
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3897 - 3914