4-溴-2,6-二硝基甲苯合成路线 （共 13 条）
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; sulfuric acid T=20°C; 1 h;
参考文献
Condon, Stephen M.; Jackson, Randy William; Laporte, Matthew G.; Burns, Christopher J.; Herbertz, Torsten; Gaboury, Janet A.
Patent: US2007/219212 A1, 2007 ;
Location in patent: Page/Page column 18 ;
反应条件
bromine; mercury(II) oxide in tetrachloromethane T=65°C; photo-Hunsdiecker reaction; 2.5 h; Irradiation;
参考文献
Boes, Michael; Sleight, Andrew J.; Godel, Thierry; Martin, James R.; Riemer, Claus; Stadler, Heinz
European Journal of Medicinal Chemistry, 2001 , vol. 36, # 2 p. 165 - 178
参考文献
US5952362 A1, ;
US 5952362 A
反应条件
1: iodine; iron; bromine / 0 °C / Lichtausschluss 2: phenol; fuming nitric acid / 0 °C 3: fuming nitric acid 4: ethanolic ammonia / 140 °C 5: Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
1: ethanolic ammonia / 140 °C 2: Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
1: phenol; fuming nitric acid / 0 °C 2: fuming nitric acid 3: ethanolic ammonia / 140 °C 4: Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
1: fuming nitric acid 2: ethanolic ammonia / 140 °C 3: Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
1: Diazotization.anschliessende Behandlung mit KBr und Brom in Eisessig 2: ethanolic ammonia / 140 °C 3: Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol View Scheme
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
Diazotization.anschliessende Behandlung mit KBr und Brom in Eisessig;
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
反应条件
Diazotization.Erwaermen der Diazoniumsalz-Loesung mit Aethanol;
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 14, # 1 p. 3,25, 26, 32, 35
