2,3-二氧代-1,2,3,4-四氢喹噁啉-6-磺酰氯合成路线 （共 3 条）
反应条件
chlorosulfonic acid
T=110°C; 8 h;
参考文献
Obafemi, Craig A.; Akinpelu
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 8 p. 1795 - 1807
反应条件
1: water / 0.07 h / Microwave irradiation
2: chlorosulfonic acid / 10 h / 0 - 20 °C
View Scheme
参考文献
Jubie, Selvaraj; Gayathri, Rajamanickam; Srividya, Ammayappan Byung; Kalirajan, Rajagopal; Prabitha, Prabakaran; Sankar, Sundaram; Elango, Kannan
Letters in Drug Design and Discovery, 2011 , vol. 8, # 4 p. 317 - 320
反应条件
1: 52 percent / aq. KMnO4; NaOH / 1 h / Heating
2: 88 percent / chlorosulfonic acid / 8 h / 110 °C
View Scheme
参考文献
Obafemi, Craig A.; Akinpelu
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 8 p. 1795 - 1807
