1-苯甲基-1,4-二氢烟酰胺合成路线 (共 156 条)
反应条件
[Ru(2,2'-bipyridine)2(CO)2](hexafluorophosphate)2; [Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in N,N-dimethyl-formamide
Irradiation (UV/VIS); irradn. (visible) of CO2 satd. dry DMF contg. Ru(bpy)3Cl2*6H2O, Ru(bpy)2(CO)2(PF6)2, BNAH; pyrex tube;
参考文献
Ishida, Hitoshi; Tanaka, Koji; Tanaka, Toshio
Chemistry Letters, 1988 , p. 339 - 342
参考文献
Sako, Magoichi; Hirota, Kosaku; Maki, Yoshifumi
Tetrahedron, 1983 , vol. 39, # 23 p. 3919 - 3922
反应条件
T=30°C; Rate constant;
参考文献
Abeles et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 712,713
反应条件
in methanol
4 h; Ambient temperature;
参考文献
Endo, Takeshi; Okawara, Makoto
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2663 - 2666
反应条件
in ethanol
T=80°C; 24 h; dark; Yield given. Yields of byproduct given;
参考文献
Oae, Shigeru; Nagata, Toshiyuki; Yoshimura, Toshiaki; Fujimori, Ken
Tetrahedron Letters, 1982 , vol. 23, # 31 p. 3189 - 3192
反应条件
in acetonitrile
T=80°C; 12 h; dark; Yield given. Yields of byproduct given;
参考文献
Oae, Shigeru; Nagata, Toshiyuki; Yoshimura, Toshiaki; Fujimori, Ken
Tetrahedron Letters, 1982 , vol. 23, # 31 p. 3189 - 3192
反应条件
in acetonitrile
T=24.84°C; KineticsActivation energy;
参考文献
Zhu, Xiao-Qing; Deng, Fei-Huang; Yang, Jin-Dong; Li, Xiu-Tao; Chen, Qiang; Lei, Nan-Ping; Meng, Fan-Kun; Zhao, Xiao-Peng; Han, Su-Hui; Hao, Er-Jun; Mu, Yuan-Yuan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6071 - 6089
反应条件
in acetonitrile
T=34.9°C; Kinetics;
参考文献
Gerresheim, W. van; Verhoeven, J. W.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 6 p. 339 - 340
反应条件
T=180°C; 3 h; examination of further 5-bromouracils, reducing compounds, solvent, temperature and reaction time; Product distributionMechanism;
参考文献
Sako, Magoichi; Hirota, Kosaku; Maki, Yoshifumi
Tetrahedron, 1983 , vol. 39, # 23 p. 3919 - 3922
反应条件
T=180°C; 3 h; examination of further 5-bromouracils, reducing compounds, solvent, temperature and reaction time; Product distributionMechanism;
参考文献
Sako, Magoichi; Hirota, Kosaku; Maki, Yoshifumi
Tetrahedron, 1983 , vol. 39, # 23 p. 3919 - 3922