sodium Yield given. Multistep reaction;

暂无反应条件数据

2: 24 percent / phosphoryl chloride / 2 h / 85 °C 3: 58 percent / 20percent methanolic ammonia / 5 h / 100 °C View Scheme

sodium ethanol; 20 deg C; 3 days;; Yield given. Multistep reaction. Yields of byproduct given;

sodium Yield given. Multistep reaction;

2: 24 percent / phosphoryl chloride / 2 h / 85 °C View Scheme

1: sodium / ethanol; 20 deg C; 3 days; 2: 95 percent / Na2CO3 / H2O / Heating 3: 87 percent / thionyl chloride / Heating 4: 98 percent / sulfur / xylene / Heating; lead tetraacetate as reagent in pyridine; 5: 96 percent / aq.NaOH / ethanol / Heating View Scheme