3-(1-苯基-1H-苯并咪唑-2-基)苯硼酸嚬哪醇酯合成路线 （共 5 条）
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane
T=80°C; 17 h; Inert atmosphere;
参考文献
NITTO DENKO CORPORATION; ZHENG, Shijun; SISK, David, T.; HARDING, Brett, T.; CAYAS, Jensen; LI, Sheng; MOCHIZUKI, Amane; CHAE, Hyun, Sik; KHAN, Sazzadur, Rahman; MA, Liping; BOTTGER, Rebecca
Patent: WO2011/34967 A1, 2011 ;
Location in patent: Page/Page column 27-28 ;
反应条件
potassium acetate in dichloromethane
参考文献
NITTO DENKO CORPORATION
Patent: US2011/62386 A1, 2011 ;
Title/Abstract Full Text Show Details
Nitto Denko Corporation
Patent: US2012/16449 A1, 2012 ;
反应条件
1.1: triethylamine / dichloromethane / 19 h / 20 °C
2.1: trichlorophosphate / 1,4-dioxane / 2 h / 115 °C
2.2: 20 °C
3.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 17 h / 80 °C / Inert atmosphere
View Scheme
参考文献
NITTO DENKO CORPORATION; ZHENG, Shijun; SISK, David, T.; HARDING, Brett, T.; CAYAS, Jensen; LI, Sheng; MOCHIZUKI, Amane; CHAE, Hyun, Sik; KHAN, Sazzadur, Rahman; MA, Liping; BOTTGER, Rebecca
Patent: WO2011/34967 A1, 2011 ;
反应条件
1.1: triethylamine / dichloromethane / 19 h / 20 °C
2.1: trichlorophosphate / 1,4-dioxane / 2 h / 115 °C
2.2: 20 °C
3.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 17 h / 80 °C / Inert atmosphere
View Scheme
参考文献
NITTO DENKO CORPORATION; ZHENG, Shijun; SISK, David, T.; HARDING, Brett, T.; CAYAS, Jensen; LI, Sheng; MOCHIZUKI, Amane; CHAE, Hyun, Sik; KHAN, Sazzadur, Rahman; MA, Liping; BOTTGER, Rebecca
Patent: WO2011/34967 A1, 2011 ;
反应条件
1.1: trichlorophosphate / 1,4-dioxane / 2 h / 115 °C
1.2: 20 °C
2.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 17 h / 80 °C / Inert atmosphere
View Scheme
参考文献
NITTO DENKO CORPORATION; ZHENG, Shijun; SISK, David, T.; HARDING, Brett, T.; CAYAS, Jensen; LI, Sheng; MOCHIZUKI, Amane; CHAE, Hyun, Sik; KHAN, Sazzadur, Rahman; MA, Liping; BOTTGER, Rebecca
Patent: WO2011/34967 A1, 2011 ;
