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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
95275-68-6
合成路线
（共 8 条）
13141-38-3
+
78-94-4
丁烯酮
→
反应条件
95275-68-6
反应条件
1: 2-(2-phenylethynyl)aniline With Li2CuCl4 in various solvent(s) T=50°C; 24 h; 2: methyl vinyl ketone in various solvent(s) T=80°C; 24 h; Further stages.;
参考文献
Ambrogio, Ilaria; Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Marinelli, Fabio
Synlett, 2007 , # 11 p. 1775 - 1779
948-65-2
2-苯基吲哚
+
78-94-4
丁烯酮
→
反应条件
95275-68-6
反应条件
palladium dichloride in acetonitrile T=60°C; Michael Addition; Inert atmosphere;
参考文献
Janreddy, Donala; Kavala, Veerababurao; Kuo, Chun-Wei; Kuo, Ting-Shen; He, Chiu-Hui; Yao, Ching-Fa
Tetrahedron, 2013 , vol. 69, # 15 p. 3323 - 3330
598-32-3
3-丁烯-2-醇
+
13141-38-3
→
反应条件
95275-68-6
反应条件
oxygen; palladium diacetate; potassium iodide in N,N-dimethyl-formamide T=90°C; P=760.051 Torr; 8 h; Reagent/catalystSolventTemperature;
参考文献
Wang, Qian; Huang, Liangbin; Wu, Xia; Jiang, Huanfeng
Organic Letters, 2013 , vol. 15, # 23 p. 5940 - 5943
849359-76-8
→
反应条件
948-65-2
2-苯基吲哚
+
95275-68-6
反应条件
Li2CuCl4 in ethanol T=140°C; 24 h;
参考文献
Alfonsi, Maria; Arcadi, Antonio; Aschi, Massimiliano; Bianchi, Gabriele; Marinelli, Fabio
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2265 - 2273
615-43-0
2-碘苯胺
→
反应条件
95275-68-6
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 20 °C / |Inert atmosphere 2: palladium diacetate; potassium iodide; oxygen / N,N-dimethyl-formamide / 8 h / 90 °C / 760.05 Torr View Scheme
参考文献
Wang, Qian; Huang, Liangbin; Wu, Xia; Jiang, Huanfeng
Organic Letters, 2013 , vol. 15, # 23 p. 5940 - 5943
536-74-3
苯乙炔
→
反应条件
95275-68-6
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 5 h / 20 °C / |Inert atmosphere 2: palladium diacetate; potassium iodide; oxygen / N,N-dimethyl-formamide / 8 h / 90 °C / 760.05 Torr View Scheme
参考文献
Wang, Qian; Huang, Liangbin; Wu, Xia; Jiang, Huanfeng
Organic Letters, 2013 , vol. 15, # 23 p. 5940 - 5943
849359-76-8
→
反应条件
95275-68-6
反应条件
1: 12 percent / NaAuCl4*2H2O / ethanol / 24 h / 140 °C 2: 42 percent / NaAuCl4*2H2O / ethanol / 24 h / 140 °C View Scheme
参考文献
Alfonsi, Maria; Arcadi, Antonio; Aschi, Massimiliano; Bianchi, Gabriele; Marinelli, Fabio
Journal of Organic Chemistry, 2005 , vol. 70, # 6 p. 2265 - 2273
13141-38-3
→
反应条件
95275-68-6
反应条件
1: 100 percent / gold catalyst / various solvent(s) / 0.17 h / 100 °C / microvawe irradiation 2: 85 percent / various solvent(s) / 24 h / 80 °C View Scheme
参考文献
Ambrogio, Ilaria; Arcadi, Antonio; Cacchi, Sandro; Fabrizi, Giancarlo; Marinelli, Fabio
Synlett, 2007 , # 11 p. 1775 - 1779
