2,3-二氢-1-苯并呋喃-7-磺酰氯合成路线 （共 3 条）
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-100°C; 1.5 h;
2: With sulfur dioxide in tetrahydrofuran
T=-100 - -85°C; 2 h;
3: With N-chloro-succinimide in dichloromethane
T=0°C; 1 h;
参考文献
Memory Pharmaceuticals Corporation
Patent: US2010/29629 A1, 2010 ;
Location in patent: Page/Page column 63 ;
US 20100029629 A1
反应条件
in 1,2-dichloro-ethane
参考文献
Corvas International, Inc.
Patent: US6541467 B1, 2003 ;
US 6541467 B1
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-100°C;
2: With sulfur dioxide in tetrahydrofuran
T=-100 - -85°C; 2 h;
3: With N-chloro-succinimide in dichloromethane
T=0°C;
参考文献
Memory Pharmaceuticals Corporation
Patent: US2010/16297 A1, 2010 ;
Location in patent: Page/Page column 34 ;
US 20100016297 A1
