5-(二氟甲氧基)-2-{[(3,4-二甲氧基-1-氧代-2-吡啶基)甲基]硫基}-1H-苯并咪唑合成路线 (共 3 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Ray, Purna C.; Mittapelli, Vasantha; Rohatgi, Amit; Tyagi, Om Dutt
Synthetic Communications, 2007 , vol. 37, # 17 p. 2861 - 2868
反应条件
1.1: sodium bicarbonate / CHCl3 1.2: 84 percent / m-chloroperbenzoic acid / 2.42 h / 5 °C 2.1: 98.44 percent / potassium carbonate / dimethylformamide / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 37, # 17 p. 2861 - 2868
反应条件
(ethylenedinitrilo)tetraacetic acid trisodium salt; ruthenium trichloride in tetrahydrofuran; 1,4-dioxane; water T=80°C; 1 h;
参考文献
Dipharma Francis S.r.l.
Patent: EP1847538 A1, 2007 ;
Location in patent: Page/Page column 6 ;