2,4,6-三甲基苯甲酮合成路线 (共 76 条)
反应条件
C4F9SO3H T=165°C; 2 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
trifluoroacetic anhydride; bismuth trifluoromethanesulphonate T=30°C; Friedel-Crafts acetylation; 12 h;
参考文献
Matsushita, Yoh-Ichi; Sugamoto, Kazuhiro; Matsui, Takanao
Tetrahedron Letters, 2004 , vol. 45, # 24 p. 4723 - 4727
反应条件
silver perchlorate; niobium pentachloride in nitromethane T=80°C; Friedel-Crafts acylation; 7 h;
参考文献
Arai, Shigeru; Sudo, Yukinori; Nishida, Atsushi
Tetrahedron, 2005 , vol. 61, # 19 p. 4639 - 4642
反应条件
sodium carbonate; palladium dichloride T=25 - 30°C; Suzuki-Miyaura type coupling reaction; 0.0833333 h;
参考文献
Bandgar; Patil
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7627 - 7630
反应条件
dipotassium peroxodisulfate; palladium diacetate in water; dimethyl sulfoxide T=20°C; 3 h;
参考文献
Li, Mingzong; Wang, Cong; Ge, Haibo
Organic Letters, 2011 , vol. 13, # 8 p. 2062 - 2064
反应条件
titanium tetrachloride in dichloromethane T=-78 - 25°C; 2 h;
参考文献
Brook, Michael A.; Henry, Courtney
Tetrahedron, 1996 , vol. 52, # 3 p. 861 - 868
反应条件
carbon in benzene 3 h; Heating;
参考文献
Kodomari, Mitsuo; Suzuki, Yoshitada; Yoshida, Kouji
Chemical Communications, 1997 , # 16 p. 1567 - 1568
反应条件
titanium tetrachloride in dichloromethane T=-78°C; 1.5 h;
参考文献
Tetrahedron, , vol. 52, # 3 p. 861 - 868
反应条件
1: AlCl3 / CS2 2: lithium dimesityl borohydride bis(dimethoxyethane) / AIBN / dimethylformamide / 61 °C / other solvent and temperature; also in a presence of DNB View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7138 - 7142
反应条件
LDPA in tetrahydrofuran T=23°C; 144 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5907 - 5914