(4S)-(+)-2,2-二甲基-1,3-二氧戊环-4- 乙酸甲酯合成路线 (共 18 条)
反应条件
toluene-4-sulfonic acid; copper(II) sulfate
参考文献
Hermitage, Stephen A.; Roberts, Stanley M.; Watson, Daniel J.
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3567 - 3570
反应条件
1: KMnO4, 18-crown-6 / benzene
View Scheme
参考文献
Papageorgiou, Christos; Benezra, Claude
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1144 - 1145
反应条件
pyridinium p-toluenesulfonate in dichloromethane
T=0°C; 1 h;
参考文献
Saito, Seiki; Hasegawa, Takashi; Inaba, Masami; Nishida, Ryosuke; Fujii, Toshikazu; et. al
Chemistry Letters, 1984 , p. 1389 - 1392
反应条件
bromine; sodium hydrogencarbonate in water
1 h; Ambient temperature; Yield given;
参考文献
Lichtenthaler, Frieder W.; Jarglis, Pan; Lorenz, Klaus
Synthesis, 1988 , # 10 p. 790 - 792
反应条件
toluene-4-sulfonic acid in acetone
0.333333 h; Ambient temperature;
参考文献
Saito; Ishikawa; Kuroda; Koga; Moriwake
Tetrahedron, 1992 , vol. 48, # 20 p. 4067 - 4086
反应条件
dimethylsulfide borane complex; toluene-4-sulfonic acid
Yield given. Multistep reaction;
参考文献
Papageorgiou, Christos; Benezra, Claude
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1144 - 1145
参考文献
Papageorgiou, Christos; Benezra, Claude
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1144 - 1145
反应条件
sodium hydride
1.) THF, 0 deg C, 5 min; Yield given. Multistep reaction;
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1994 , vol. 47, # 9 p. 1661 - 1672