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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
95460-42-7
合成路线
(共 6 条)
95460-42-7
→
反应条件
68236-23-7
2-氯-6,7-二甲氧基-3-喹啉甲醛
反应条件
dicyclohexyl-carbodiimide; pyridinium chlorochromate in chloroform T=30°C; 0.5 h;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1286 - 1287
95460-42-7
→
反应条件
93299-56-0
2-氯-6,7-二甲氧基-3-喹啉甲腈
反应条件
thionyl chloride in benzene 3 h; Heating;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A.P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 431 - 434
95460-42-7
→
反应条件
93299-58-2
+
93347-84-3
+
93299-57-1
+
93299-56-0
2-氯-6,7-二甲氧基-3-喹啉甲腈
反应条件
potassium carbonate; epichlorohydrin in methanol 3 h; Heating; Further byproducts given;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A.P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 431 - 434
95460-42-7
+
106-89-8
环氧氯丙烷
→
反应条件
93299-58-2
+
93347-84-3
+
93299-57-1
+
93299-56-0
2-氯-6,7-二甲氧基-3-喹啉甲腈
反应条件
potassium carbonate in methanol 3 h; Heating; Further byproducts given;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A.P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 431 - 434
67-56-1
甲醇
+
95460-42-7
+
106-89-8
环氧氯丙烷
→
反应条件
93347-84-3
+
93299-57-1
+
93299-59-3
+
93299-56-0
2-氯-6,7-二甲氧基-3-喹啉甲腈
反应条件
potassium carbonate in methanol 3 h; Heating; Further byproducts given;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A.P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 431 - 434
67-56-1
甲醇
+
95460-42-7
→
反应条件
93299-58-2
+
93347-84-3
+
93299-57-1
+
93299-56-0
2-氯-6,7-二甲氧基-3-喹啉甲腈
反应条件
potassium carbonate; epichlorohydrin 3 h; Heating; Further byproducts given;
参考文献
Bhat, Neelima Balkrishen; Bhaduri, A.P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 431 - 434