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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
955-24-8
合成路线
（共 8 条）
188559-42-4
→
反应条件
955-24-8
反应条件
trifluoroacetic acid in dichloromethane
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
103285-11-6
→
反应条件
955-24-8
反应条件
acetic acid in water T=90°C; 0.5 h;
参考文献
Srivastav, Naveen C.; Shakya, Neeraj; Mak, Michelle; Agrawal, Babita; Tyrrell, D. Lorne; Kumar, Rakesh
Journal of Medicinal Chemistry, 2010 , vol. 53, # 19 p. 7156 - 7166
134485-31-7
→
反应条件
955-24-8
反应条件
1: diisopropylethylamine 2: K2OsO4*2H2O, K3Fe(CN)6, DHQD-PHN / H2O; 2-methyl-propan-2-ol 3: H2SO4 / tetrahydrofuran / 0 °C 4: 80 percent / NaH / dimethylformamide 5: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating 6: 28 percent / pyridine*HF / dioxane 7: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
134485-39-5
→
反应条件
955-24-8
反应条件
1: DIBAL-H / diethyl ether / -78 °C 2: diisopropylethylamine 3: K2OsO4*2H2O, K3Fe(CN)6, DHQD-PHN / H2O; 2-methyl-propan-2-ol 4: H2SO4 / tetrahydrofuran / 0 °C 5: 80 percent / NaH / dimethylformamide 6: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating 7: 28 percent / pyridine*HF / dioxane 8: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
188559-08-2
→
反应条件
955-24-8
反应条件
1: K2OsO4*2H2O, K3Fe(CN)6, DHQD-PHN / H2O; 2-methyl-propan-2-ol 2: H2SO4 / tetrahydrofuran / 0 °C 3: 80 percent / NaH / dimethylformamide 4: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating 5: 28 percent / pyridine*HF / dioxane 6: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
188559-39-9
→
反应条件
955-24-8
反应条件
1: 28 percent / pyridine*HF / dioxane 2: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
188559-34-4
→
反应条件
955-24-8
反应条件
1: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating 2: 28 percent / pyridine*HF / dioxane 3: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
188559-11-7
→
反应条件
955-24-8
反应条件
1: H2SO4 / tetrahydrofuran / 0 °C 2: 80 percent / NaH / dimethylformamide 3: 84 percent / Rh(PPh3)3Cl, pyridine / aq. ethanol / 5 h / Heating 4: 28 percent / pyridine*HF / dioxane 5: 86 percent / 50percent TFA / CH2Cl2 View Scheme
参考文献
Xia, Xiaoyang; Wang, Jianying; Hager, Michael W.; Sisti, Nicholas; Liotta, Dennis C.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1111 - 1114
