N2-甲基-4-硝基-1,2-苯二胺合成路线 （共 7 条）
反应条件
sodium carbonate in N,N-dimethyl-formamide
18 h;
参考文献
SCHICKANEDER, Helmut; SCHICKANEDER, Christian; BUSCHAUER, Armin; BERNHARDT, Günther; HUBER, Stefan; LIMMERT, Michael; LUBBE, Mathias; HOFMEIER, Harald
Patent: WO2013/189847 A1, 2013 ;
Location in patent: Page/Page column 25; 30; 31 ;
反应条件
sulfuric acid
T=130°C;
参考文献
Leandri et al.
Gazzetta Chimica Italiana, 1955 , vol. 85, p. 769,788
反应条件
ammonia; water
T=160°C;
参考文献
Phillips
Journal of the Chemical Society, 1931 , p. 1143,1153
反应条件
2: water; ammonia / 160 °C
View Scheme
参考文献
Phillips
Journal of the Chemical Society, 1931 , p. 1143,1153
反应条件
1: water; NH3 / 210 °C
2: H2SO4 / 130 °C
View Scheme
参考文献
Leandri et al.
Gazzetta Chimica Italiana, 1955 , vol. 85, p. 769,788
反应条件
PPA in xylene
T=60 - 150°C;
参考文献
Richards, Mark L.; Lio, Shirley Cruz; Sinha, Anjana; Banie, Homayon; Thomas, Richard J.; Major, Michael; Tanji, Mark; Sircar, Jagadish C.
European Journal of Medicinal Chemistry, 2006 , vol. 41, # 8 p. 950 - 969
参考文献
Leandri et al.
Gazzetta Chimica Italiana, 1955 , vol. 85, p. 769,788
