2-甲基-3-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苯甲酸甲酯合成路线 (共 2 条)
反应条件
potassium phosphate; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane T=100°C; 72 h;
参考文献
EP2011788 A1, ;
Page/Page column 19 ;
反应条件
1.1: sulfuric acid / 22 h / Reflux 1.2: pH 7 - 8 2.1: potassium acetate / triphenylphosphine; [RuCl2(=CHPh)(PPh3)2] / 1,4-dioxane / 20 - 100 °C / Inert atmosphere View Scheme